5-Azido-1,4-diphenyl-1,2,3-triazole

Base Information

• Chemical Name: 5-Azido-1,4-diphenyl-1,2,3-triazole
• CAS No.: 32364-53-7
• Molecular Formula: C₁₄H₁₀N₆
• Molecular Weight: 262.274
• Mol file: 32364-53-7.mol

Synonyms:

Chemical Property of 5-Azido-1,4-diphenyl-1,2,3-triazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-Azido-1,4-diphenyl-1,2,3-triazole

There total 1 articles about 5-Azido-1,4-diphenyl-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 5-Azido-1,4-diphenyl-1,2,3-triazole (32364-53-7)

Guidance literature:

1,4-Diphenyl-5-amino-triazol-(1,2,3), Natriumazid, Diazotierung;

DOI:10.1021/ja01064a024

Reference yield:

5-Azido-1,4-diphenyl-1,2,3-triazole (32364-53-7) → 1-Benzoyl-3-phenyltriazene (29411-28-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1,2-dichloro-ethane / 52 °C / also other temperatures (40.0 and 64.4 deg C); activation energy

2: 42 percent / 50percent aq. NaOH / petroleum ether; diethyl ether; acetone; H₂O / Ambient temperature

With sodium hydroxide; In diethyl ether; water; 1,2-dichloro-ethane; acetone; Petroleum ether;

DOI:10.1021/jo00297a066

Reference yield:

5-Azido-1,4-diphenyl-1,2,3-triazole (32364-53-7) → 1-Phenyl-3-(α-cyanobenzylidene)triazene (126159-17-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1,2-dichloro-ethane / 52 °C / also other temperatures (40.0 and 64.4 deg C); activation energy

2: 70 percent / Na₂S₂O₄ / H₂O; acetone / 0 h / Ambient temperature

With sodium dithionite; In water; 1,2-dichloro-ethane; acetone;

DOI:10.1021/jo00297a066

Downstream raw materials:

(5-amino-3,4-diphenyl-pyrrol-2-ylidene)-phenyl-amine

diphenylmaleimide

1-Benzoyl-3-phenyltriazene

1-Phenyl-3-(α-cyanobenzylidene)triazene