2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-ribo-hept-3-enononitril

Base Information

Chemical Name:2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-ribo-hept-3-enononitril
CAS No.:126257-50-9
Molecular Formula:C₂₇H₃₇NO₃
Molecular Weight:423.596
Hs Code.:

2,6-Anhydro-5-O-<4'-<trans-4''-(n-heptyl)cyclohexyl>benzoyl>-3,4,7-tridesoxy-L-ribo-hept-3-enononitril

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Chemical Property of 2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-ribo-hept-3-enononitril

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Technology Process of 2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-ribo-hept-3-enononitril

There total 4 articles about 2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-ribo-hept-3-enononitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 81930-19-0
trans-4-(4-Heptylcyclohexyl)benzoesaeurechlorid

: 126257-49-6
2,6-Anhydro-3,4,7-tridesoxy-L-ribo-hept-3-enononitril

: 126257-50-9
2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-ribo-hept-3-enononitril

Guidance literature:: With pyridine; for 1h;

Reference yield:

: 34819-86-8
3,4-di-O-acetyl-6-deoxy-L-glucal

: 126257-50-9
2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-ribo-hept-3-enononitril

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / Et₂O*BF₃ / acetonitrile / 0.17 h

2: 1) AcCl 2) conc. HCl / 1) MeOH, r.t.

3: 18 percent / pyridine / 1 h

With pyridine; hydrogenchloride; boron trifluoride diethyl etherate; acetyl chloride; In acetonitrile;

Reference yield:

: 65355-31-9
4'-benzoesaeure

: 126257-50-9
2,6-Anhydro-5-O-<4'-benzoyl>-3,4,7-tridesoxy-L-ribo-hept-3-enononitril

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂, DMF / 1 h / Ambient temperature

2: 18 percent / pyridine / 1 h

With pyridine; thionyl chloride; N,N-dimethyl-formamide;