3,5-dioctadecyl-4,6-dichloro-1,2-benzoquinone

Base Information

Chemical Name:3,5-dioctadecyl-4,6-dichloro-1,2-benzoquinone
CAS No.:74061-24-8
Molecular Formula:C₄₂H₇₄Cl₂O₂
Molecular Weight:681.954
Hs Code.:

Synonyms:

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Chemical Property of 3,5-dioctadecyl-4,6-dichloro-1,2-benzoquinone

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Technology Process of 3,5-dioctadecyl-4,6-dichloro-1,2-benzoquinone

There total 6 articles about 3,5-dioctadecyl-4,6-dichloro-1,2-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 74061-23-7
3,5-dioctadecylpyrocatechol

: 74061-24-8
3,5-dioctadecyl-4,6-dichloro-1,2-benzoquinone

Guidance literature:: With sulfuryl dichloride; for 0.05h; Heating;

Reference yield:

: 1177-44-2
4-stearoylpyrocatechol

: 74061-24-8
3,5-dioctadecyl-4,6-dichloro-1,2-benzoquinone

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / N₂H₄*H₂O, KOH, Na₂SO₃ / bis-(2-hydroxy-ethyl) ether / 1.) 150 deg C, 1 h; 2.) 195 deg C, 4 h

2: 89 percent / BF₃ / 6 h / 160 °C

3: 85 percent / BF₃ etherate, triethylsilane / trifluoroacetic acid / 6 h / 55 - 60 °C

4: 73 percent / SO₂Cl₂ / 0.05 h / Heating

With triethylsilane; potassium hydroxide; sulfuryl dichloride; boron trifluoride diethyl etherate; boron trifluoride; hydrazine hydrate; sodium sulfite; In trifluoroacetic acid; diethylene glycol;

Reference yield:

: 1170-77-0
4-octadecyl-pyrocatechol

: 74061-24-8
3,5-dioctadecyl-4,6-dichloro-1,2-benzoquinone

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / BF₃ / 6 h / 160 °C

2: 85 percent / BF₃ etherate, triethylsilane / trifluoroacetic acid / 6 h / 55 - 60 °C

3: 73 percent / SO₂Cl₂ / 0.05 h / Heating

With triethylsilane; sulfuryl dichloride; boron trifluoride diethyl etherate; boron trifluoride; In trifluoroacetic acid;