Bis(3-hydroxy-4-caranyl) suldide

Base Information

• Chemical Name: Bis(3-hydroxy-4-caranyl) suldide
• CAS No.: 135028-46-5
• Molecular Formula: C₂₀H₃₄O₂S
• Molecular Weight: 338.555
• Mol file: 135028-46-5.mol

Synonyms:

Chemical Property of Bis(3-hydroxy-4-caranyl) suldide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Bis(3-hydroxy-4-caranyl) suldide

There total 4 articles about Bis(3-hydroxy-4-caranyl) suldide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

3-carene epoxide (936-91-4) → β-benzylthiocaran-3α-ol (134927-26-7) + Bis(3α-hydroxycaran-4β-yl) Sulfide (135028-46-5)

Guidance literature:

With sodium ethanolate; S-benzylisothiourea hydrochloride; In ethanol; for 30h; Heating;

Reference yield: 8.0%

S-benzylisothiourea hydrochloride (538-28-3,860511-29-1) + 3-carene epoxide (936-91-4) → β-benzylthiocaran-3α-ol (134927-26-7) + Bis(3α-hydroxycaran-4β-yl) Sulfide (135028-46-5)

Guidance literature:

With sodium ethanolate; In ethanol; for 30h; Heating;

Reference yield:

(1S,3R,4S,6R)-3,4-epoxycarane (936-91-4,936-92-5,2225-98-1,21218-11-1,35671-18-2) → Bis(3-hydroxy-4-caranyl) suldide (85392-33-2,135028-46-5,135028-49-8,138232-97-0,138232-98-1)

Guidance literature:

With sodium ethanolate; thiourea; In ethanol; Yield given; Heating;

upstream raw materials:

S-benzylisothiourea hydrochloride

3-carene epoxide

(1S,3R,4S,6R)-3,4-epoxycarane

α-3,4-Epoxycarane