(S)-2-((S)-3-Carboxy-2-{2-[2-(2,4-dinitro-phenylamino)-acetylamino]-acetylamino}-propionylamino)-5-guanidino-pentanoic acid; compound with trifluoro-acetic acid

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Chemical Name:(S)-2-((S)-3-Carboxy-2-{2-[2-(2,4-dinitro-phenylamino)-acetylamino]-acetylamino}-propionylamino)-5-guanidino-pentanoic acid; compound with trifluoro-acetic acid
CAS No.:88830-95-9
Molecular Formula:C₂HF₃O₂*C₂₀H₂₇N₉O₁₁
Molecular Weight:683.512
Hs Code.:

(S)-2-((S)-3-Carboxy-2-{2-[2-(2,4-dinitro-phenylamino)-acetylamino]-acetylamino}-propionylamino)-5-guanidino-pentanoic acid; compound with trifluoro-acetic acid

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Chemical Property of (S)-2-((S)-3-Carboxy-2-{2-[2-(2,4-dinitro-phenylamino)-acetylamino]-acetylamino}-propionylamino)-5-guanidino-pentanoic acid; compound with trifluoro-acetic acid

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Technology Process of (S)-2-((S)-3-Carboxy-2-{2-[2-(2,4-dinitro-phenylamino)-acetylamino]-acetylamino}-propionylamino)-5-guanidino-pentanoic acid; compound with trifluoro-acetic acid

There total 5 articles about (S)-2-((S)-3-Carboxy-2-{2-[2-(2,4-dinitro-phenylamino)-acetylamino]-acetylamino}-propionylamino)-5-guanidino-pentanoic acid; compound with trifluoro-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 88830-93-7
(S)-2-((S)-3-tert-Butoxycarbonyl-2-{2-[2-(2,4-dinitro-phenylamino)-acetylamino]-acetylamino}-propionylamino)-5-guanidino-pentanoic acid

: 88830-95-9
(S)-2-((S)-3-Carboxy-2-{2-[2-(2,4-dinitro-phenylamino)-acetylamino]-acetylamino}-propionylamino)-5-guanidino-pentanoic acid; compound with trifluoro-acetic acid

Guidance literature:: With trifluoroacetic acid; In diethyl ether; for 1h;
DOI:10.1007/BF00575711

Reference yield:

: β-tert-butyl ester of aspartyl arginine

: 88830-95-9
(S)-2-((S)-3-Carboxy-2-{2-[2-(2,4-dinitro-phenylamino)-acetylamino]-acetylamino}-propionylamino)-5-guanidino-pentanoic acid; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / dimethylformamide / 48 h / Ambient temperature

2: 66 percent / CF₃COOH / diethyl ether / 1 h

With trifluoroacetic acid; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1007/BF00575711

Reference yield:

: (S)-2-((S)-3-tert-Butoxycarbonyl-2-tert-butoxycarbonylamino-propionylamino)-5-guanidino-pentanoic acid; compound with methanol

: 88830-95-9
(S)-2-((S)-3-Carboxy-2-{2-[2-(2,4-dinitro-phenylamino)-acetylamino]-acetylamino}-propionylamino)-5-guanidino-pentanoic acid; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 85percent formic acid / 1 h

2: 57 percent / dimethylformamide / 48 h / Ambient temperature

3: 66 percent / CF₃COOH / diethyl ether / 1 h

With formic acid; trifluoroacetic acid; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1007/BF00575711