C₃₀H₃₄O₄Se

Base Information

• Chemical Name: C₃₀H₃₄O₄Se
• CAS No.: 79782-39-1
• Molecular Formula: C₃₀H₃₄O₄Se
• Molecular Weight: 537.558
• Mol file: 79782-39-1.mol

Synonyms:

Chemical Property of C₃₀H₃₄O₄Se

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₃₄O₄Se

There total 6 articles about C₃₀H₃₄O₄Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2S,4aS,5R,8R,8aS)-5,8-Bis-benzyloxy-3-phenylselanyl-decahydro-naphthalen-2-ol (79782-38-0,84173-24-0) → C30H34O4Se (79782-39-1,84173-25-1)

Guidance literature:

With dihydrogen peroxide; In tetrahydrofuran; at 25 ℃; for 2.5h;

DOI:10.1021/ja00411a063

Reference yield:

Phenylselenyl bromide (34837-55-3) → C30H34O4Se (79782-39-1,84173-25-1)

Guidance literature:

Multi-step reaction with 3 steps

1: KOAc / 1 h / 25 °C

2: 89 percent / KOH / methanol; diethyl ether / 2 h / 25 °C

3: H₂O₂ / tetrahydrofuran / 2.5 h / 25 °C

With potassium hydroxide; dihydrogen peroxide; potassium acetate; In tetrahydrofuran; methanol; diethyl ether;

DOI:10.1021/ja00411a063

Reference yield:

(+/-)-1,4,5,8,9,10-trans-hexahydronaphthalene-1,4-dione (2906-93-6,3198-51-4,6102-42-7,36159-09-8,54963-84-7,84275-37-6) → C30H34O4Se (79782-39-1,84173-25-1)

Guidance literature:

Multi-step reaction with 5 steps

1: 33 percent / Aureobasidium pullulans NRRL Y-12610

2: 99 percent / NaH / dimethylsulfoxide / 25 °C

3: KOAc / 1 h / 25 °C

4: 89 percent / KOH / methanol; diethyl ether / 2 h / 25 °C

5: H₂O₂ / tetrahydrofuran / 2.5 h / 25 °C

With potassium hydroxide; Aureobasidium pullulans NRRL Y-12610; dihydrogen peroxide; potassium acetate; sodium hydride; In tetrahydrofuran; methanol; diethyl ether; dimethyl sulfoxide;

DOI:10.1021/ja00411a063

upstream raw materials:

(2S,4aS,5R,8R,8aS)-5,8-Bis-benzyloxy-3-phenylselanyl-decahydro-naphthalen-2-ol

Phenylselenyl bromide

(+/-)-1,4,5,8,9,10-trans-hexahydronaphthalene-1,4-dione

(-)-(1S,4S,9R)-Δ⁶-trans-Octalin-1,4-diol

Downstream raw materials:

(4aS,5R,8R,8aS)-5,8-Bis-benzyloxy-1,2,4a,5,6,7,8,8a-octahydro-naphthalen-2-ol

mevastatin

1β,4α-bis(benzyloxy)-7-oxo-1,2,3,4,4aβ,7,8,8aα-octahydronaphthalene

3,5-Dihydroxy-7-[(1S,2S,8S,8aR)-2-methyl-8-((S)-2-methyl-butyryloxy)-1,2,6,7,8,8a-hexahydro-naphthalen-1-yl]-heptanoic acid methyl ester