4-cyanophenyltriphenylphosphonium iodide

Base Information

• Chemical Name: 4-cyanophenyltriphenylphosphonium iodide
• CAS No.: 38182-05-7
• Molecular Formula: C₂₅H₁₉NP*I
• Molecular Weight: 491.311
• Mol file: 38182-05-7.mol

Synonyms:

Chemical Property of 4-cyanophenyltriphenylphosphonium iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-cyanophenyltriphenylphosphonium iodide

There total 2 articles about 4-cyanophenyltriphenylphosphonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

4-iodobenzonitrile (3058-39-7) + triphenylphosphine (603-35-0) → 4-cyanophenyltriphenylphosphonium iodide (38182-05-7)

Guidance literature:

palladium diacetate;

DOI:10.1039/DT9880000277

Reference yield:

4-Aminobenzonitrile (873-74-5) → 4-cyanophenyltriphenylphosphonium iodide (38182-05-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / sodium iodide / various solvent(s) / 0 °C

2: 20 percent / palladium acetate

With sodium iodide; palladium diacetate; In various solvent(s);

DOI:10.1039/DT9880000277

Reference yield:

4-cyanophenyltriphenylphosphonium iodide (38182-05-7) → C25H19NP(1+)*FH*F(1-)

Guidance literature:

With HF₂^- containing resin column;

DOI:10.1039/DT9880000277

upstream raw materials:

4-iodobenzonitrile

triphenylphosphine

4-Aminobenzonitrile

Downstream raw materials:

(4-Cyano-phenyl)-triphenyl-phosphonium; fluoride