N-[(8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-10,13-dimethyl-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-cyclopenta[a]phenanthren-(3Z)-ylidene]-N'-(2,4-dinitro-phenyl)-hydrazine

Base Information

• Chemical Name: N-[(8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-10,13-dimethyl-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-cyclopenta[a]phenanthren-(3Z)-ylidene]-N'-(2,4-dinitro-phenyl)-hydrazine
• CAS No.: 33432-99-4
• Molecular Formula: C₃₃H₄₆N₄O₄
• Molecular Weight: 562.753

Synonyms:

Chemical Property of N-[(8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-10,13-dimethyl-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-cyclopenta[a]phenanthren-(3Z)-ylidene]-N'-(2,4-dinitro-phenyl)-hydrazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Useful:

Technology Process of N-[(8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-10,13-dimethyl-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-cyclopenta[a]phenanthren-(3Z)-ylidene]-N'-(2,4-dinitro-phenyl)-hydrazine

There total 2 articles about N-[(8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-10,13-dimethyl-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-cyclopenta[a]phenanthren-(3Z)-ylidene]-N'-(2,4-dinitro-phenyl)-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cholesta-1,4-dien-3-one (566-91-6) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → N-[(8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-10,13-dimethyl-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-cyclopenta[a]phenanthren-(3Z)-ylidene]-N'-(2,4-dinitro-phenyl)-hydrazine (33432-99-4)

Guidance literature:

With phosphoric acid; In ethanol;

DOI:10.1016/S0040-4020(01)97753-1

Reference yield:

cholesta-1,4-dien-3-one (566-91-6) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → cholesta-1,4-dien-3-one-(2,4-dinitro-phenylhydrazone) (33432-99-4)

Guidance literature:

Reference yield:

N-[(8S,9S,10R,13R,14S,17R)-17-((R)-1,5-Dimethyl-hexyl)-10,13-dimethyl-6,7,8,9,10,11,12,13,14,15,16,17-dodecahydro-cyclopenta[a]phenanthren-(3Z)-ylidene]-N'-(2,4-dinitro-phenyl)-hydrazine (33432-99-4) + trifluoroacetic anhydride (407-25-0) → Trifluoro-acetic acid N-[(8S,9S,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-4,13-dimethyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-1-yl]-N'-(2,4-dinitro-phenyl)-hydrazide (33433-00-0)

Guidance literature:

In tetrachloromethane; Heating;

DOI:10.1016/S0040-4020(01)97753-1

upstream raw materials:

cholesta-1,4-dien-3-one

(2,4-dinitro-phenyl)-hydrazine

Downstream raw materials:

Trifluoro-acetic acid N-[(8S,9S,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-4,13-dimethyl-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-1-yl]-N'-(2,4-dinitro-phenyl)-hydrazide

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