2-{1-[(E)-3-(4-Chloro-phenyl)-5-mercapto-[1,2,4]triazol-4-ylimino]-ethyl}-phenol

Base Information

Chemical Name:2-{1-[(E)-3-(4-Chloro-phenyl)-5-mercapto-[1,2,4]triazol-4-ylimino]-ethyl}-phenol
CAS No.:930807-50-4
Molecular Formula:C₁₆H₁₃ClN₄OS
Molecular Weight:344.824
Hs Code.:

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Chemical Property of 2-{1-[(E)-3-(4-Chloro-phenyl)-5-mercapto-[1,2,4]triazol-4-ylimino]-ethyl}-phenol

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Technology Process of 2-{1-[(E)-3-(4-Chloro-phenyl)-5-mercapto-[1,2,4]triazol-4-ylimino]-ethyl}-phenol

There total 1 articles about 2-{1-[(E)-3-(4-Chloro-phenyl)-5-mercapto-[1,2,4]triazol-4-ylimino]-ethyl}-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 68468-95-1
4-amino-5-mercapto-3-(4-chlorophenyl)-1,2,4-triazole

: 930807-50-4
2-{1-[(E)-3-(4-Chloro-phenyl)-5-mercapto-[1,2,4]triazol-4-ylimino]-ethyl}-phenol

Guidance literature:: In ethanol;

Reference yield: 60.0%

: 930807-50-4
2-{1-[(E)-3-(4-Chloro-phenyl)-5-mercapto-[1,2,4]triazol-4-ylimino]-ethyl}-phenol

: cobalt(II) chloride hexahydrate

: [Co(C₂N₃(C₆H₄Cl)SNC(CH₃)C₆H₄O)(H₂O)2Cl]

Guidance literature:: With H₂O₂; In ethanol; by refluxing ethanolic soln. of a ligand (0.01 mol) with CoCl2*6H2O (0.01 mol); addn. of H2O2 (30%); the solid was filtered off, washed with cold ethanol, and dried over anhyd. CaCl2; elem. anal.;

Reference yield: 55.0%

: 930807-50-4
2-{1-[(E)-3-(4-Chloro-phenyl)-5-mercapto-[1,2,4]triazol-4-ylimino]-ethyl}-phenol

: 121714-78-1,24290-40-2,58694-80-7,10025-77-1,64333-00-2
iron(III) chloride hexahydrate

: [Fe(C₂N₃(C₆H₄Cl)SNC(CH₃)C₆H₄O)(H₂O)2Cl]

Guidance literature:: With KOH; In ethanol; to a soln. of a ligand (0.01 mol) in EtOH was added FeCl3*6H2O (0.01 mol) dropwise with stirring; pH 8-9 (satd. soln. of KOH); warming on a water bath for 1 h; the complex was filtered, washed with distd. water, aq. ethanol and finally with ether and dried in a desiccator at room temp.; elem. anal.;