C₃₃H₄₄F₃N₃O₆

Base Information

Chemical Name:C₃₃H₄₄F₃N₃O₆
CAS No.:1601475-93-7
Molecular Formula:C₃₃H₄₄F₃N₃O₆
Molecular Weight:635.724
Hs Code.:

C<sub>33</sub>H<sub>44</sub>F<sub>3</sub>N<sub>3</sub>O<sub>6</sub>

Synonyms:

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Chemical Property of C₃₃H₄₄F₃N₃O₆

Chemical Property:

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Technology Process of C₃₃H₄₄F₃N₃O₆

There total 8 articles about C₃₃H₄₄F₃N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₂₁NO

: 1601475-93-7
C₃₃H₄₄F₃N₃O₆

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen; 10 wt% Pd(OH)2 on carbon

2: sodium hydroxide / tetrahydrofuran

3: Dess-Martin periodane

4: 0 - 40 °C

5: HATU; N-ethyl-N,N-diisopropylamine

With 10 wt% Pd(OH)2 on carbon; hydrogen; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; HATU; sodium hydroxide; In tetrahydrofuran; 4: |Bargellini Reaction;
DOI:10.1016/j.bmcl.2014.02.055

Reference yield:

: 5,5-dimethyl-piperidin-3-ol

: 1601475-93-7
C₃₃H₄₄F₃N₃O₆

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / tetrahydrofuran

2: Dess-Martin periodane

3: 0 - 40 °C

4: HATU; N-ethyl-N,N-diisopropylamine

With Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; HATU; sodium hydroxide; In tetrahydrofuran; 3: |Bargellini Reaction;
DOI:10.1016/j.bmcl.2014.02.055

Reference yield:

: 103201-79-2,103667-54-5,118918-76-6,1820583-17-2
(3R,7aS)-3-Phenyl-tetrahydro-pyrrolo[1,2-c]oxazol-5-one

: 1601475-93-7
C₃₃H₄₄F₃N₃O₆

Guidance literature:: Multi-step reaction with 8 steps

1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / Reflux

3: trifluoroacetic anhydride; triethylamine / 96 h / -78 - 60 °C

4: hydrogen; 10 wt% Pd(OH)2 on carbon

5: sodium hydroxide / tetrahydrofuran

6: Dess-Martin periodane

7: 0 - 40 °C

8: HATU; N-ethyl-N,N-diisopropylamine

With lithium aluminium tetrahydride; 10 wt% Pd(OH)2 on carbon; hydrogen; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic anhydride; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; 7: |Bargellini Reaction;
DOI:10.1016/j.bmcl.2014.02.055