C₁₁H₁₃NO

Base Information

• Chemical Name: C₁₁H₁₃NO
• CAS No.: 1611477-39-4
• Molecular Formula: C₁₁H₁₃NO
• Molecular Weight: 175.23
• Mol file: 1611477-39-4.mol

Synonyms:

Chemical Property of C₁₁H₁₃NO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₁H₁₃NO

There total 3 articles about C₁₁H₁₃NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C11H12ClNO (1611477-30-5) → C11H13NO (1611477-39-4)

Guidance literature:

With tert-butyl isocyanide; CpRu(PiPr₃)(CH₃CN)2PF₆; Dimethylphenylsilane; In dichloromethane-d2; at 20 ℃; for 1.5h; Schlenk technique;

DOI:10.1039/c4dt00372a

Reference yield:

N-(3-acetylphenyl)propionamide → C11H13NO (1611477-39-4)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus pentachloride / dichloromethane / 1 h / 20 °C / Schlenk technique

2: Dimethylphenylsilane; CpRu(PiPr₃)(CH₃CN)2PF₆; tert-butyl isocyanide / dichloromethane-d2 / 1.5 h / 20 °C / Schlenk technique

With tert-butyl isocyanide; CpRu(PiPr₃)(CH₃CN)2PF₆; phosphorus pentachloride; Dimethylphenylsilane; In dichloromethane; dichloromethane-d2;

DOI:10.1039/c4dt00372a

Reference yield:

1-(3-aminophenyl)ethanone (99-03-6) → C11H13NO (1611477-39-4)

Guidance literature:

Multi-step reaction with 3 steps

1: dichloromethane / 20 °C / Schlenk technique

2: phosphorus pentachloride / dichloromethane / 1 h / 20 °C / Schlenk technique

3: Dimethylphenylsilane; CpRu(PiPr₃)(CH₃CN)2PF₆; tert-butyl isocyanide / dichloromethane-d2 / 1.5 h / 20 °C / Schlenk technique

With tert-butyl isocyanide; CpRu(PiPr₃)(CH₃CN)2PF₆; phosphorus pentachloride; Dimethylphenylsilane; In dichloromethane; dichloromethane-d2;

DOI:10.1039/c4dt00372a

upstream raw materials:

1-(3-aminophenyl)ethanone

C₁₁H₁₂ClNO