(+/-)-Psilostachyin

Base Information

Chemical Name:(+/-)-Psilostachyin
CAS No.:64813-80-5
Molecular Formula:C₁₅H₂₀O₄
Molecular Weight:264.321
Hs Code.:

Synonyms:

Suppliers and Price of (+/-)-Psilostachyin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-Psilostachyin

Chemical Property:

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Safty Information:

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Technology Process of (+/-)-Psilostachyin

There total 14 articles about (+/-)-Psilostachyin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 60133-11-1
rac-damsin

: 6466-67-7,64813-80-5
(+/-)-Psilostachyin

Guidance literature:: With bis-trimethylsilanyl peroxide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - -50 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jo2001275

Reference yield:

: C₁₉H₃₀O₄

: 6466-67-7,64813-80-5
(+/-)-Psilostachyin

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 100 °C / Sealed tube; Inert atmosphere

2: hydrogenchloride / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

3: bis-trimethylsilanyl peroxide; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 24 h / -78 - -50 °C / Inert atmosphere

With hydrogenchloride; bis-trimethylsilanyl peroxide; trimethylsilyl trifluoromethanesulfonate; sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil; 3: Baeyer-Villiger oxidation;
DOI:10.1021/jo2001275

Reference yield:

: C₂₀H₃₀O₄

: 6466-67-7,64813-80-5
(+/-)-Psilostachyin

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

2: bis-trimethylsilanyl peroxide; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 24 h / -78 - -50 °C / Inert atmosphere

With hydrogenchloride; bis-trimethylsilanyl peroxide; trimethylsilyl trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane; 2: Baeyer-Villiger oxidation;
DOI:10.1021/jo2001275