1,4-Dihydro-6-methoxy-7-nitroquinoxaline-2,3-dione

Base Information

Chemical Name:1,4-Dihydro-6-methoxy-7-nitroquinoxaline-2,3-dione
CAS No.:69399-57-1
Molecular Formula:C₉H₇N₃O₅
Molecular Weight:237.172
Hs Code.:
European Community (EC) Number:614-960-9
DSSTox Substance ID:DTXSID801036402

Synonyms:1,4-Dihydro-6-methoxy-7-nitroquinoxaline-2,3-dione;69399-57-1;SCHEMBL6108125;DTXSID801036402;NS00003671;6-methoxy-7-nitro-1,4-dihydroquinoxaline-2,3-dione

Suppliers and Price of 1,4-Dihydro-6-methoxy-7-nitroquinoxaline-2,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
1,4-dihydro-6-methoxy-7-nitro-2,3-Quinoxalinedione 97.00%
25G
$ 5520.00

AccelPharmtech
1,4-dihydro-6-methoxy-7-nitro-2,3-Quinoxalinedione 97.00%
5G
$ 2960.00

AccelPharmtech
1,4-dihydro-6-methoxy-7-nitro-2,3-Quinoxalinedione 97.00%
1G
$ 1740.00

Total 2 raw suppliers

Chemical Property of 1,4-Dihydro-6-methoxy-7-nitroquinoxaline-2,3-dione

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Density:1.673g/cm3 at 23℃
XLogP3:0.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:237.03857033
Heavy Atom Count:17
Complexity:366

Purity/Quality:

99.9% ^*data from raw suppliers

1,4-dihydro-6-methoxy-7-nitro-2,3-Quinoxalinedione 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C2C(=C1)NC(=O)C(=O)N2)[N+](=O)[O-]

Technology Process of 1,4-Dihydro-6-methoxy-7-nitroquinoxaline-2,3-dione

There total 3 articles about 1,4-Dihydro-6-methoxy-7-nitroquinoxaline-2,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 68836-14-6
6-methoxy-7-nitro-quinoxaline

: 69399-57-1
6-methoxy-7-nitroquinoxaline-2,3-dione

Guidance literature:: With water; bis-[(trifluoroacetoxy)iodo]benzene; In acetonitrile; at 20 ℃; for 24h;
DOI:10.1021/jo401872e

Reference yield: 75.0%

: 31910-18-6
2,3-dioxo-6-methoxy-1,2,3,4-tetrahydroquinoxaline

: 69399-57-1
6-methoxy-7-nitroquinoxaline-2,3-dione

Guidance literature:: With sulfuric acid; potassium nitrate; 1) 0 deg C, 30 min, 2) RT, 4 h;

Reference yield:

: 96-96-8
4-methoxy-2-nitroaniline

: 69399-57-1
6-methoxy-7-nitroquinoxaline-2,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: iron; hydrogenchloride / water; ethanol / 80 °C / pH 7-8 / Inert atmosphere

1.2: 95 °C / Inert atmosphere

2.1: nitric acid / 70 - 90 °C

With hydrogenchloride; nitric acid; iron; In ethanol; water;