6Rsv8EG2QE

Base Information

• Chemical Name: 6Rsv8EG2QE
• CAS No.: 83608-70-2
• Molecular Formula: C₁₆H₁₅ClN₂O₂
• Molecular Weight: 302.76
• UNII: 6RSV8EG2QE
• Nikkaji Number: J459.206I

Synonyms:6RSV8EG2QE;UNII-6RSV8EG2QE;Tetrazepam impurity A [EP];2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-1-methyl-5-(3-oxo-1-cyclohexen-1-yl)-;7-Chloro-1,3-dihydro-1-methyl-5-(3-oxo-1-cyclohexen-1-yl)-2H-1,4-benzodiazepin-2-one;83608-70-2;TETRAZEPAM IMPURITY A [EP IMPURITY]

Chemical Property of 6Rsv8EG2QE

Chemical Property:

• XLogP3: 1.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 302.0822054
• Heavy Atom Count: 21
• Complexity: 526

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN1C(=O)CN=C(C2=C1C=CC(=C2)Cl)C3=CC(=O)CCC3

Technology Process of 6Rsv8EG2QE

There total 1 articles about 6Rsv8EG2QE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrazepam (10379-14-3) → 7-chloro-5-(3-keto-1-cyclohexen-1-yl)-1,3-dihydro-1-methyl-2H-1,4-benzodiazepin-2-one (83608-70-2) + 7-chloro-5-(3-hydroperoxy-1-cyclohexen-1-yl)-1,3-dihydro-1-methyl-2H-1,4-benzodiazepin-2-one (142780-67-4) + 7-chloro-5-(1,2-epoxycyclohexan-1-yl)-1,3-dihydro-1-methyl-2H-1,4-benzodiazepin-2-one (142780-68-5) + 7-chloro-1-methyl-3,4-dihydro-1H-1,4-benzodiazepine-2,5-dione (5973-28-4)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); oxygen; In acetonitrile; at 40 ℃; for 48h; Product distribution; Mechanism; var. reagents, solvents, times and temperatures;

DOI:10.1002/jps.2600810216

upstream raw materials:

tetrazepam

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