sodium salt of 6--2,2-dimethylpenam-3-carboxylic acid

Base Information

Chemical Name:sodium salt of 6--2,2-dimethylpenam-3-carboxylic acid
CAS No.:90687-01-7
Molecular Formula:C₂₆H₂₂N₃O₇S*Na
Molecular Weight:543.532
Hs Code.:

sodium salt of 6-<N-(1H-2-benzopyran-1-onyl-3-carbonyl)-2R-2-aminophenylacetamide>-2,2-dimethylpenam-3-carboxylic acid

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Chemical Property of sodium salt of 6--2,2-dimethylpenam-3-carboxylic acid

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Technology Process of sodium salt of 6--2,2-dimethylpenam-3-carboxylic acid

There total 2 articles about sodium salt of 6--2,2-dimethylpenam-3-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2289-03-4
1-oxo-1H-isochromene-3-carboxylic acid

: 90687-01-7
sodium salt of 6--2,2-dimethylpenam-3-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride

2: hexamethyldisilazane, triethyl amine / 1)methylene chloride, reflux 2)-5 deg C,reaction with chloride of acid 3)room temp., 1h

With thionyl chloride; triethylamine; 1,1,1,3,3,3-hexamethyl-disilazane;
DOI:10.1007/BF00515632

Reference yield:

: 90686-93-4
1-oxo-1H-isochromene-3-carbonyl chloride

: 33993-48-5
ampicillin

: 90687-01-7
sodium salt of 6--2,2-dimethylpenam-3-carboxylic acid

Guidance literature:: With triethylamine; 1,1,1,3,3,3-hexamethyl-disilazane; Yield given. Multistep reaction; 1)methylene chloride, reflux 2)-5 deg C,reaction with chloride of acid 3)room temp., 1h;
DOI:10.1007/BF00515632