Technology Process of sodium 3-hydroxy-4-methoxy-1,3,5,(10)-estatriene-17-one 3-sulfate
There total 5 articles about sodium 3-hydroxy-4-methoxy-1,3,5,(10)-estatriene-17-one 3-sulfate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfur trioxide pyridine complex;
In
pyridine;
for 12h;
ice-cooling;
DOI:10.1248/cpb.30.4417
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 650 mg / CdCO3 / benzene / 10 h / Heating
2: 36 mg / diethyl ether; CHCl3 / 12 h / Ambient temperature
3: 12 mg / 1n NaOH / methanol / 12 h / Ambient temperature
4: Helix pomatia / H2O / 24 h / 37 °C / 0.1 M acetate buffer (pH=4.7)
5: 46 mg / sulfur trioxide-pyridine complex / pyridine / 12 h / ice-cooling
With
sodium hydroxide; cadmium(II) carbonate; Helix pomatia; sulfur trioxide pyridine complex;
In
pyridine; methanol; diethyl ether; chloroform; water; benzene;
DOI:10.1248/cpb.30.4417
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 36 mg / diethyl ether; CHCl3 / 12 h / Ambient temperature
2: 12 mg / 1n NaOH / methanol / 12 h / Ambient temperature
3: Helix pomatia / H2O / 24 h / 37 °C / 0.1 M acetate buffer (pH=4.7)
4: 46 mg / sulfur trioxide-pyridine complex / pyridine / 12 h / ice-cooling
With
sodium hydroxide; Helix pomatia; sulfur trioxide pyridine complex;
In
pyridine; methanol; diethyl ether; chloroform; water;
DOI:10.1248/cpb.30.4417
