Technology Process of C19H28N2O6
There total 6 articles about C19H28N2O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydrogencarbonate / water; tetrahydrofuran; dichloromethane / 7 h / 60 °C
2: Resolution of racemate
With
sodium hydrogencarbonate;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1021/acs.jmedchem.7b00377
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetic acid; zinc / water; ethanol / 0.67 h / 20 °C
2: sodium hydrogencarbonate / water; tetrahydrofuran; dichloromethane / 7 h / 60 °C
3: Resolution of racemate
With
sodium hydrogencarbonate; acetic acid; zinc;
In
tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/acs.jmedchem.7b00377
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thionyl chloride / 192 h / 70 - 75 °C
2: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 60 °C
3: acetic acid; zinc / water; ethanol / 0.67 h / 20 °C
4: sodium hydrogencarbonate / water; tetrahydrofuran; dichloromethane / 7 h / 60 °C
5: Resolution of racemate
With
thionyl chloride; sodium hydrogencarbonate; acetic acid; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; zinc;
In
tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/acs.jmedchem.7b00377
