Technology Process of 2-chloro-5-methylhexane
There total 4 articles about 2-chloro-5-methylhexane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
at 0 ℃;
und mehrwoechigen Aufbewahren im Druckgefaess bei 20grad;
DOI:10.1021/ja01276a066
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) n-nonane, manganese stearate, 2.) LiAlH4 / 1.) 125 deg C, 10 h, 2.) THF, reflux, 1 h
2: thionyl chloride, pyridine
With
pyridine; lithium aluminium tetrahydride; thionyl chloride; nonane; manganese(II) stearate;
DOI:10.1002/prac.19943360109
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) O2, 2.) aq. H2SO4 / 1.) diethyl ether, -65 deg C
2: 1.) n-nonane, manganese stearate, 2.) LiAlH4 / 1.) 125 deg C, 10 h, 2.) THF, reflux, 1 h
3: thionyl chloride, pyridine
With
pyridine; lithium aluminium tetrahydride; thionyl chloride; nonane; sulfuric acid; oxygen; manganese(II) stearate;
DOI:10.1002/prac.19943360109