5-ethoxy-3-methoxy-2-methyl-aniline

Base Information

• Chemical Name: 5-ethoxy-3-methoxy-2-methyl-aniline
• CAS No.: 856343-47-0
• Molecular Formula: C₁₀H₁₅NO₂
• Molecular Weight: 181.235
• Mol file: 856343-47-0.mol

Synonyms:

Chemical Property of 5-ethoxy-3-methoxy-2-methyl-aniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-ethoxy-3-methoxy-2-methyl-aniline

There total 5 articles about 5-ethoxy-3-methoxy-2-methyl-aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-ethoxy-2-methoxy-6-nitro-toluene (21859-73-4) → 5-ethoxy-3-methoxy-2-methyl-aniline (856343-47-0)

Guidance literature:

With sodium sulfide; ethanol;

DOI:10.1039/jr9330000819

Reference yield:

2,6-dinitro-4-hydroxytoluene (63989-82-2) → 5-ethoxy-3-methoxy-2-methyl-aniline (856343-47-0)

Guidance literature:

Multi-step reaction with 5 steps

1: K₂CO₃; acetone

2: tin (II)-chloride; hydrogen chloride; ethanol

4: aqueous KOH

5: sodium sulfide; aqueous ethanol

With hydrogenchloride; sodium sulfide; potassium hydroxide; ethanol; potassium carbonate; acetone; tin(ll) chloride;

DOI:10.1039/jr9330000819

Reference yield:

5-ethoxy-2-methyl-3-nitro-aniline (21913-56-4) → 5-ethoxy-3-methoxy-2-methyl-aniline (856343-47-0)

Guidance literature:

Multi-step reaction with 3 steps

2: aqueous KOH

3: sodium sulfide; aqueous ethanol

With sodium sulfide; potassium hydroxide; ethanol;

DOI:10.1039/jr9330000819

upstream raw materials:

4-ethoxy-2-methoxy-6-nitro-toluene

2,6-dinitro-4-hydroxytoluene

5-ethoxy-2-methyl-3-nitro-aniline

5-ethoxy-2-methyl-3-nitro-phenol

Downstream raw materials:

5-ethoxy-3-methoxy-2-methyl-phenol

1-(6-ethoxy-2-hydroxy-4-methoxy-3-methyl-phenyl)-butan-1-one