(+)-(S)-Melochinin

Base Information

Chemical Name:(+)-(S)-Melochinin
CAS No.:83542-30-7
Molecular Formula:C₁₉H₃₃NO₃
Molecular Weight:323.476
Hs Code.:

Synonyms:

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Chemical Property of (+)-(S)-Melochinin

Chemical Property:

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Technology Process of (+)-(S)-Melochinin

There total 3 articles about (+)-(S)-Melochinin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83542-34-1
(+)-(S)-6-(11-Hydroxydodecyl)-3-methoxy-2-methyl-4-pyron

: 83542-30-7,70001-21-7
(+)-(S)-Melochinin

Guidance literature:: With ammonium hydroxide; In methanol; at 100 ℃; for 48h;
DOI:10.1002/jlac.198219820806

Reference yield:

: 83515-81-5,83542-32-9,83542-33-0
(+)-(S)-6-(11-Hydroxy-1-dodecen-1-yl)-3-methoxy-2-methyl-4-pyron

: 83542-30-7,70001-21-7
(+)-(S)-Melochinin

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10 percent Pd/C / methanol / 0.33 h

2: 6 M NH₃ / methanol / 48 h / 100 °C

With ammonium hydroxide; hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1002/jlac.198219820806

Reference yield:

: 83515-79-1,83515-80-4
(+)-(S)-6-(2,11-Dihydroxydodecyl)-3-methoxy-2-methyl-4-pyron

: 83542-30-7,70001-21-7
(+)-(S)-Melochinin

Guidance literature:: Multi-step reaction with 3 steps

1: p-toluenesulfonic acid-hydrate / toluene / 0.75 h / 150 - 155 °C

2: H₂ / 10 percent Pd/C / methanol / 0.33 h

3: 6 M NH₃ / methanol / 48 h / 100 °C

With ammonium hydroxide; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; toluene;
DOI:10.1002/jlac.198219820806