2,3-dimethylhexadecane

Base Information

• Chemical Name: 2,3-dimethylhexadecane
• CAS No.: 61868-02-8
• Molecular Formula: C₁₈H₃₈
• Molecular Weight: 254.5
• Mol file: 61868-02-8.mol

Synonyms:

Chemical Property of 2,3-dimethylhexadecane

Chemical Property:

• Vapor Pressure: 0.000964mmHg at 25°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-dimethylhexadecane

There total 4 articles about 2,3-dimethylhexadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Pedicellinsaeure (6803-77-6) → Pedicellan (61868-02-8)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂SO₄ / benzene / Heating

2: LiAlH₄ / dimethyl ether / Heating

3: (i) I₂, P, (ii) LiAlH₄, Et₂O

With lithium aluminium tetrahydride; sulfuric acid; In Dimethyl ether; benzene;

DOI:10.1016/S0040-4020(01)99448-7

Reference yield:

2-methyl-3-tridecyl-succinic acid dimethyl ester (94874-43-8) → Pedicellan (61868-02-8)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄ / dimethyl ether / Heating

2: (i) I₂, P, (ii) LiAlH₄, Et₂O

With lithium aluminium tetrahydride; In Dimethyl ether;

DOI:10.1016/S0040-4020(01)99448-7

Reference yield:

3-methyl-butan-2-one (563-80-4) + tridecylmagnesium bromide (117711-00-9) → Pedicellan (61868-02-8)

Guidance literature:

With diethyl ether; und Erhitzen des Reaktionsprodukts mit Naphthalin-2-sulfonsaeure auf 110grad und Hydrieren des erhaltenen Olefin-Gemisches an Raney-Nickel bei 190grad/200 at;

upstream raw materials:

3-methyl-butan-2-one

tridecylmagnesium bromide

2-methyl-3-tridecyl-butane-1,4-diol

Pedicellinsaeure