(Z)-apoisoquinidine

Base Information

• Chemical Name: (Z)-apoisoquinidine
• CAS No.: 60801-73-2
• Molecular Formula: C₂₀H₂₄N₂O₂
• Molecular Weight: 324.423
• Mol file: 60801-73-2.mol

Synonyms:

Chemical Property of (Z)-apoisoquinidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z)-apoisoquinidine

There total 4 articles about (Z)-apoisoquinidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

quinidine → (Z)-Δ3,10-isoquinidine (60801-73-2,697260-51-8) + (E)-Δ3,10-isoquinidine (697260-51-8)

Guidance literature:

With hydrogenchloride; 10 percent palladium on barium sulphate; In ethanol; water; at 85 ℃; for 0.833333h; Reagent/catalyst; Overall yield = 96 %; Overall yield = 2.84 g; Microwave irradiation;

DOI:10.1007/s10562-017-2169-3

Reference yield:

quinidine (1234784-40-7) → (Z)-Δ3,10-isoquinidine (60801-73-2,697260-51-8) + (E)-Δ3,10-isoquinidine (697260-51-8)

Guidance literature:

With hydrogenchloride; Rh/Al₂O₃; In ethanol; for 24h; Heating;

DOI:10.1016/S0040-4039(03)01180-8

Reference yield:

→ Apo-epi-Chinidin (16934-07-9,16934-08-0,55399-64-9,60801-73-2,139237-97-1,697260-51-8)

Guidance literature:

α-Brom (oder α-Chlor)-dihydro-epichinidin, KOH;

upstream raw materials:

quinidine