C₂₆H₃₈O₇

Base Information

• Chemical Name: C₂₆H₃₈O₇
• CAS No.: 82210-23-9
• Molecular Formula: C₂₆H₃₈O₇
• Molecular Weight: 462.584
• Mol file: 82210-23-9.mol

Synonyms:

Chemical Property of C₂₆H₃₈O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₃₈O₇

There total 3 articles about C₂₆H₃₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-acetoxy-17-hydroxy-16β,23-epoxy-21,24-dinorchola-5,22(23)-dien-20-one (76768-93-9,82950-85-4) → C26H38O7 (82210-23-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) NaBH₄, 2) pyridine / 1) aq.DMF, 20 h, 2) pyridine

2: 180 mg / m-chloroperoxybenzoic acid / CH₂Cl₂ / 72 h / 20 °C

With pyridine; sodium tetrahydroborate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1007/BF00581598

Reference yield:

3β,20β-diacetoxy-17α-hydroxy-16β,23-epoxy-21,24-dinorchol-5-ene (82210-13-7,82730-44-7,82950-87-6) → C26H38O7 (82210-23-9)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 72h;

DOI:10.1007/BF00581598

Reference yield:

3β-acetoxy-16β,23-oxido-21,24-dinorchol-5-en-17α-ol-20-one (55898-59-4,82263-32-9,82950-86-5) → C26H38O7 (82210-23-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) NaBH₄, 2) pyridine / 1) aq.DMF, 20 deg C, 3.5 h, 2) pyridine

2: 180 mg / m-chloroperoxybenzoic acid / CH₂Cl₂ / 72 h / 20 °C

With pyridine; sodium tetrahydroborate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1007/BF00581598

upstream raw materials:

3β,20β-diacetoxy-17α-hydroxy-16β,23-epoxy-21,24-dinorchol-5-ene

3β-acetoxy-16β,23-oxido-21,24-dinorchol-5-en-17α-ol-20-one

3-acetoxy-17-hydroxy-16β,23-epoxy-21,24-dinorchola-5,22(23)-dien-20-one