di<1-(p-nitrophenyl)propargyl>ether

Base Information Edit

Chemical Name:di<1-(p-nitrophenyl)propargyl>ether
CAS No.:123772-72-5
Molecular Formula:C₁₈H₁₂N₂O₅
Molecular Weight:336.304
Hs Code.:
Mol file:123772-72-5.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di<1-(p-nitrophenyl)propargyl>ether Edit

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Technology Process of di<1-(p-nitrophenyl)propargyl>ether

There total 2 articles about di<1-(p-nitrophenyl)propargyl>ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

: 78725-73-2
1-(4-Nitro-phenyl)-2-propyn-1-ol

: 75-05-8,26809-02-9
acetonitrile

: 123772-67-8
N-<1-(4-nitrophenyl)-2-propynyl>acetamide

: 123772-72-5,123783-76-6
di<1-(p-nitrophenyl)propargyl>ether

Guidance literature:: With sulfuric acid; sodium sulfate; for 1.5h; Heating;

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 123772-72-5,123783-76-6
di<1-(p-nitrophenyl)propargyl>ether

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / 1.) hexane, THF, -78 deg C, 3h, 2.) -78 deg C, 5h

2: 6 percent / Na₂SO₄, 96percent sulfuric acid / 1.5 h / Heating

With n-butyllithium; sulfuric acid; sodium sulfate;