tert-butyl morpholine-2-carboxylate

Base Information

Chemical Name:tert-butyl morpholine-2-carboxylate
CAS No.:664364-75-4
Molecular Formula:C₉H₁₇NO₃
Molecular Weight:187.239
Hs Code.:
Mol file:664364-75-4.mol

Synonyms:

Suppliers and Price of tert-butyl morpholine-2-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
[1,2]Oxazinane-2-carboxylicAcidtert-ButylEster
50mg
$ 45.00

Chemenu
tert-Butyl1,2-oxazinane-2-carboxylate 95%
5g
$ 631.00

Alichem
tert-Butylmorpholine-2-carboxylate
5g
$ 696.90

Alichem
tert-Butylmorpholine-2-carboxylate
1g
$ 250.70

AK Scientific
tert-butyloxazinane-2-carboxylate
25g
$ 1878.80

AK Scientific
tert-butyloxazinane-2-carboxylate
250mg
$ 165.20

Total 2 raw suppliers

Chemical Property of tert-butyl morpholine-2-carboxylate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

[1,2]Oxazinane-2-carboxylicAcidtert-ButylEster ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tert-butyl morpholine-2-carboxylate

There total 3 articles about tert-butyl morpholine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 110-52-1
1,4-dibromo-butane

: 36016-38-3
tert-Butyl N-hydroxycarbamate

: 664364-75-4
tert-butyl 1,2-oxazinane-2-carboxylate

Guidance literature:: With potassium hydroxide; In ethanol; at 60 ℃; for 6h; Inert atmosphere;
DOI:10.1055/s-0036-1588480

Reference yield:

: 147462-15-5
tert-butyl 3,6-dihydrooxazine-2-carboxylate

: 664364-75-4
tert-butyl 1,2-oxazinane-2-carboxylate

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In methanol; under 760.051 Torr;
DOI:10.1055/a-1683-0484

Reference yield:

: 36016-38-3
tert-Butyl N-hydroxycarbamate

: 664364-75-4
tert-butyl 1,2-oxazinane-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: copper dichloride; 2-ethyl-4,5-dihydrooxazole; oxygen / tetrahydrofuran; dichloromethane; methanol / 18 h

2: hydrogen; 5%-palladium/activated carbon / methanol / 760.05 Torr

With 2-ethyl-4,5-dihydrooxazole; 5%-palladium/activated carbon; hydrogen; oxygen; copper dichloride; In tetrahydrofuran; methanol; dichloromethane; 1: |Diels-Alder Cycloaddition;
DOI:10.1055/a-1683-0484