Sulfuric acid mono-{2-[2,23-dimethyl-22-(2-sulfooxy-ethoxymethyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-dibenzo[a,c]cycloeicosen-3-ylmethoxy]-ethyl} ester; compound with pyridine

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Chemical Name:Sulfuric acid mono-{2-[2,23-dimethyl-22-(2-sulfooxy-ethoxymethyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-dibenzo[a,c]cycloeicosen-3-ylmethoxy]-ethyl} ester; compound with pyridine
CAS No.:79154-91-9
Molecular Formula:2C₅H₅N*C₃₀H₄₄O₁₆S₂
Molecular Weight:883.005
Hs Code.:

Sulfuric acid mono-{2-[2,23-dimethyl-22-(2-sulfooxy-ethoxymethyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-dibenzo[a,c]cycloeicosen-3-ylmethoxy]-ethyl} ester; compound with pyridine

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Chemical Property of Sulfuric acid mono-{2-[2,23-dimethyl-22-(2-sulfooxy-ethoxymethyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-dibenzo[a,c]cycloeicosen-3-ylmethoxy]-ethyl} ester; compound with pyridine

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Technology Process of Sulfuric acid mono-{2-[2,23-dimethyl-22-(2-sulfooxy-ethoxymethyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-dibenzo[a,c]cycloeicosen-3-ylmethoxy]-ethyl} ester; compound with pyridine

There total 2 articles about Sulfuric acid mono-{2-[2,23-dimethyl-22-(2-sulfooxy-ethoxymethyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-dibenzo[a,c]cycloeicosen-3-ylmethoxy]-ethyl} ester; compound with pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 79154-92-0
4,4'-bis(2'-hydroxyethoxymethyl)-5,5'-dimethylbiphenyl-20-crown-6

: 79154-91-9
Sulfuric acid mono-{2-[2,23-dimethyl-22-(2-sulfooxy-ethoxymethyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-dibenzo[a,c]cycloeicosen-3-ylmethoxy]-ethyl} ester; compound with pyridine

Guidance literature:: In benzene; at 60 ℃; for 0.5h;
DOI:10.1016/S0040-4020(01)97950-5

Reference yield:

: 79154-98-6
4,4'-bis(chloromethyl)-5,5'-dimethylbiphenyl-20-crown-6

: 79154-91-9
Sulfuric acid mono-{2-[2,23-dimethyl-22-(2-sulfooxy-ethoxymethyl)-6,7,9,10,12,13,15,16,18,19-decahydro-5,8,11,14,17,20-hexaoxa-dibenzo[a,c]cycloeicosen-3-ylmethoxy]-ethyl} ester; compound with pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaOH / 1.) 50 deg C, 1 h, 2.) room temperature, 48 h

2: 71 percent / benzene / 0.5 h / 60 °C

With sodium hydroxide; In benzene;
DOI:10.1016/S0040-4020(01)97950-5