5β-Cholestane-3α,7α,12α,25-tetraol tetraacetate

Base Information

• Chemical Name: 5β-Cholestane-3α,7α,12α,25-tetraol tetraacetate
• CAS No.: 60354-50-9
• Molecular Formula: C₃₅H₅₆O₈
• Molecular Weight: 604.825
• Mol file: 60354-50-9.mol

Synonyms:

Chemical Property of 5β-Cholestane-3α,7α,12α,25-tetraol tetraacetate

Chemical Property:

• Boiling Point: 609.3±55.0 °C(Predicted)
• Density: 1.11±0.1 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5β-Cholestane-3α,7α,12α,25-tetraol tetraacetate

There total 3 articles about 5β-Cholestane-3α,7α,12α,25-tetraol tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cholic acid (7170-94-7) → 5β-cholestanetetrayl-(3α,7α,12α,25)-tetraacetate (60354-50-9)

Guidance literature:

Multi-step reaction with 3 steps

1: diethyl ether; methanol

2: benzene

3: pyridine

With pyridine; methanol; diethyl ether; benzene;

DOI:10.1021/ja01198a066

Reference yield:

3α,7α,12α-trihydroxy-5β-cholane-24-carboxylic acid methyl ester (59445-12-4) → 5β-cholestanetetrayl-(3α,7α,12α,25)-tetraacetate (60354-50-9)

Guidance literature:

Multi-step reaction with 2 steps

1: benzene

2: pyridine

With pyridine; benzene;

DOI:10.1021/ja01198a066

Reference yield:

5β-Cholestane-3α,7α,12α,25-tetrol (18866-87-0) + acetic anhydride (108-24-7) → 5β-cholestanetetrayl-(3α,7α,12α,25)-tetraacetate (60354-50-9)

Guidance literature:

With pyridine;

DOI:10.1021/ja01198a066

upstream raw materials:

5β-Cholestane-3α,7α,12α,25-tetrol

acetic anhydride

cholic acid

3α,7α,12α-trihydroxy-5β-cholane-24-carboxylic acid methyl ester