cyano-2 bicyclo(4.4.0) decane trans

Base Information

• Chemical Name: cyano-2 bicyclo(4.4.0) decane trans
• CAS No.: 6240-40-0
• Molecular Formula: C₁₁H₁₇N
• Molecular Weight: 163.263
• Mol file: 6240-40-0.mol

Synonyms:

Chemical Property of cyano-2 bicyclo(4.4.0) decane trans

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cyano-2 bicyclo(4.4.0) decane trans

There total 4 articles about cyano-2 bicyclo(4.4.0) decane trans which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans-1-decalone (21370-71-8) → cyano-2 bicyclo(4.4.0) decane trans (6240-40-0,6240-41-1,78549-80-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 3.0 g / CHCl₃; ethanol; acetic acid / 2 h / Ambient temperature

2: oxychlorure de phosphore / pyridine / 5 h / Heating

3: 2.0 g / H₂ / Pd/C / acetic acid; ethyl acetate / 20 h

With oxychlorure de phosphore; hydrogen; palladium on activated charcoal; In pyridine; ethanol; chloroform; acetic acid; ethyl acetate;

DOI:10.1016/S0040-4020(01)97658-6

Reference yield:

cyano-2 bicyclo(4.4.0)decanol-2 trans (4711-66-4) → cyano-2 bicyclo(4.4.0) decane trans (6240-40-0,6240-41-1,78549-80-1)

Guidance literature:

Multi-step reaction with 2 steps

1: oxychlorure de phosphore / pyridine / 5 h / Heating

2: 2.0 g / H₂ / Pd/C / acetic acid; ethyl acetate / 20 h

With oxychlorure de phosphore; hydrogen; palladium on activated charcoal; In pyridine; acetic acid; ethyl acetate;

DOI:10.1016/S0040-4020(01)97658-6

Reference yield:

2,3,4,4a,5,6,7,8-ocatahydronaphthalene-1-carbonitrile (78525-79-8) + cyano-2 bicyclo(4.4.0) decene-2 trans (78525-80-1) → cyano-2 bicyclo(4.4.0) decane trans (6240-40-0,6240-41-1,78549-80-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In acetic acid; ethyl acetate; for 20h;

DOI:10.1016/S0040-4020(01)97658-6

upstream raw materials:

(+/-)-1ξ-Cyan-(4arH,8atH)-decahydro-1ξ-naphthoesaeure

2,3,4,4a,5,6,7,8-ocatahydronaphthalene-1-carbonitrile

cyano-2 bicyclo(4.4.0) decene-2 trans

trans-1-decalone

Downstream raw materials:

(+/-)-(4ar,8at)-decahydro-[1t]naphthoic acid