(4E)-4-({2-[4-(diphenylmethyl)piperazin-1-yl]ethyl}imino)-2,6-dimethyl-3-nitropyridin-1(4H)-ol trihydrochloride

Base Information

Chemical Name:(4E)-4-({2-[4-(diphenylmethyl)piperazin-1-yl]ethyl}imino)-2,6-dimethyl-3-nitropyridin-1(4H)-ol trihydrochloride
CAS No.:110629-23-7
Molecular Formula:C₂₆H₃₁N₅O₃*3ClH
Molecular Weight:570.947
Hs Code.:

Synonyms:1-Piperazineethanamine,N-(2,6-dimethyl-3-nitro-1-oxido-4-pyridinyl)-4-(diphenylmethyl)-,trihydrochloride (9CI); 1-Piperazineethanamine,N-(2,6-dimethyl-3-nitro-4-pyridinyl)-4-(diphenylmethyl)-, N-oxide,trihydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4E)-4-({2-[4-(diphenylmethyl)piperazin-1-yl]ethyl}imino)-2,6-dimethyl-3-nitropyridin-1(4H)-ol trihydrochloride

Chemical Property:

Vapor Pressure:2.31E-13mmHg at 25°C
Boiling Point:559.7°C at 760 mmHg
Flash Point:292.3°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (4E)-4-({2-[4-(diphenylmethyl)piperazin-1-yl]ethyl}imino)-2,6-dimethyl-3-nitropyridin-1(4H)-ol trihydrochloride

There total 2 articles about (4E)-4-({2-[4-(diphenylmethyl)piperazin-1-yl]ethyl}imino)-2,6-dimethyl-3-nitropyridin-1(4H)-ol trihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 841-77-0
diphenylmethylpiperazine

: 110629-57-7
4-<(2-chloroethyl)amino>-2,6-dimethyl-3-nitropyridine-1-oxide

: 110629-23-7
[2-(4-Benzhydryl-piperazin-1-yl)-ethyl]-(2,6-dimethyl-3-nitro-1-oxy-pyridin-4-yl)-amine; hydrochloride

Guidance literature:: With hydrogenchloride; triethylamine; In N,N-dimethyl-formamide; for 2h; Heating;
DOI:10.1016/0223-5234(89)90003-2

Reference yield:

: 20185-62-0
4-chloro-2,6-dimethyl-3-nitropyridine-1-oxide

: 110629-23-7
[2-(4-Benzhydryl-piperazin-1-yl)-ethyl]-(2,6-dimethyl-3-nitro-1-oxy-pyridin-4-yl)-amine; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / propan-2-ol / 20 h / Heating

2: 22 percent / 1.) triethylamine; 2.) ethanolic HCl / dimethylformamide / 2 h / Heating

With hydrogenchloride; triethylamine; In N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1016/0223-5234(89)90003-2