ICI 118551

Base Information

• Chemical Name: ICI 118551
• CAS No.: 72795-23-4
• Molecular Formula: C₁₇H₂₇NO₂
• Molecular Weight: 277.407
• Mol file: 72795-23-4.mol

Synonyms:

Chemical Property of ICI 118551

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ICI 118551

There total 2 articles about ICI 118551 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-[((E)-But-2-enyl)oxy]-7-methyl-indan → ICI 118551 (72795-17-6,72795-19-8,72795-20-1,72795-23-4,72795-26-7,91021-57-7,149021-76-1,149115-13-9,149115-14-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) NBS, 2) DBU / 1) DME, H₂O, 24 h, 2) DME, 6 h

2: methanol

With N-Bromosuccinimide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol;

DOI:10.1071/C98145

Reference yield:

isopropylamine (75-31-0) + 2-methyl-3-(7-methylindan-4-yloxymethyl)oxirane → ICI 118551 (72795-17-6,72795-19-8,72795-20-1,72795-23-4,72795-26-7,91021-57-7,149021-76-1,149115-13-9,149115-14-0)

Guidance literature:

In methanol;

DOI:10.1071/C98145

upstream raw materials:

isopropylamine