C₁₀H₁₇NO

Base Information

Chemical Name:C₁₀H₁₇NO
CAS No.:1358526-95-0
Molecular Formula:C₁₀H₁₇NO
Molecular Weight:167.251
Hs Code.:

Synonyms:

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Chemical Property of C₁₀H₁₇NO

Chemical Property:

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Technology Process of C₁₀H₁₇NO

There total 13 articles about C₁₀H₁₇NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1358526-82-5
C₃₄H₅₁NO₅SSi

: 1358526-95-0
C₁₀H₁₇NO

Guidance literature:: Multi-step reaction with 9 steps

1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium iodide / 1,2-dimethoxyethane / 3 h / 80 °C

2: hexane; toluene / 2 h / 0 - 20 °C

3: 20 % Pd(OH)2/C; hydrogen / methanol / 12 h / 20 °C / 7600.51 Torr / Autoclave

4: potassium carbonate / tetrahydrofuran; water / 1 h / 0 °C

5: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C

6: Jones reagent / acetone / 1 h / 0 - 20 °C

7: ethyl acetate / 0.5 h / 0 °C

8: palladium on activated charcoal; hydrogen / methanol / 1 h / 20 °C

9: toluene / 5 h / Reflux

With hydrogenchloride; Jones reagent; 2,2'-azobis(isobutyronitrile); palladium on activated charcoal; 20 % Pd(OH)2/C; hydrogen; tri-n-butyl-tin hydride; potassium carbonate; sodium iodide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; hexane; water; ethyl acetate; acetone; toluene; 6: Jones oxidation;
DOI:10.1021/jo202350z

Reference yield:

: C₂₉H₄₃NO₄Si

: 1358526-95-0
C₁₀H₁₇NO

Guidance literature:: Multi-step reaction with 12 steps

1: hydrogen / ethanol / 2 h / 20 °C

2: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 2 h / 0 °C

3: dmap; triethylamine / dichloromethane / 2 h / 20 °C

4: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium iodide / 1,2-dimethoxyethane / 3 h / 80 °C

5: hexane; toluene / 2 h / 0 - 20 °C

6: 20 % Pd(OH)2/C; hydrogen / methanol / 12 h / 20 °C / 7600.51 Torr / Autoclave

7: potassium carbonate / tetrahydrofuran; water / 1 h / 0 °C

8: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C

9: Jones reagent / acetone / 1 h / 0 - 20 °C

10: ethyl acetate / 0.5 h / 0 °C

11: palladium on activated charcoal; hydrogen / methanol / 1 h / 20 °C

12: toluene / 5 h / Reflux

With hydrogenchloride; dmap; Jones reagent; 2,2'-azobis(isobutyronitrile); palladium on activated charcoal; 20 % Pd(OH)2/C; hydrogen; tri-n-butyl-tin hydride; potassium carbonate; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; sodium iodide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; hexane; dichloromethane; water; ethyl acetate; acetone; toluene; 9: Jones oxidation;
DOI:10.1021/jo202350z

Reference yield:

: C₂₉H₄₃NO₄Si

: 1358526-95-0
C₁₀H₁₇NO

Guidance literature:: Multi-step reaction with 13 steps

1: deuterated DMF / 1.5 h / 70 °C

2: hydrogen / ethanol / 2 h / 20 °C

3: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene / 2 h / 0 °C

4: dmap; triethylamine / dichloromethane / 2 h / 20 °C

5: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium iodide / 1,2-dimethoxyethane / 3 h / 80 °C

6: hexane; toluene / 2 h / 0 - 20 °C

7: 20 % Pd(OH)2/C; hydrogen / methanol / 12 h / 20 °C / 7600.51 Torr / Autoclave

8: potassium carbonate / tetrahydrofuran; water / 1 h / 0 °C

9: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C

10: Jones reagent / acetone / 1 h / 0 - 20 °C

11: ethyl acetate / 0.5 h / 0 °C

12: palladium on activated charcoal; hydrogen / methanol / 1 h / 20 °C

13: toluene / 5 h / Reflux

With hydrogenchloride; dmap; Jones reagent; 2,2'-azobis(isobutyronitrile); palladium on activated charcoal; 20 % Pd(OH)2/C; hydrogen; tri-n-butyl-tin hydride; potassium carbonate; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; sodium iodide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; ethanol; hexane; dichloromethane; deuterated DMF; water; ethyl acetate; acetone; toluene; 10: Jones oxidation;
DOI:10.1021/jo202350z