4-bromo-2-(4-bromo-phenoxy)-aniline

Base Information

• Chemical Name: 4-bromo-2-(4-bromo-phenoxy)-aniline
• CAS No.: 873980-35-9
• Molecular Formula: C₁₂H₉Br₂NO
• Molecular Weight: 343.018
• Mol file: 873980-35-9.mol

Synonyms:

Chemical Property of 4-bromo-2-(4-bromo-phenoxy)-aniline

Chemical Property:

• Boiling Point: 366.4±37.0 °C(Predicted)
• Density: 1.762±0.06 g/cm3(Predicted)

Purity/Quality:

98% ^*data from raw suppliers

4-Bromo-2-(4-bromophenoxy)aniline 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-bromo-2-(4-bromo-phenoxy)-aniline

There total 10 articles about 4-bromo-2-(4-bromo-phenoxy)-aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetic acid-[4-bromo-2-(4-bromo-phenoxy)-anilide] (873386-17-5) → 4-bromo-2-(4-bromo-phenoxy)-aniline (873980-35-9)

Guidance literature:

With hydrogenchloride;

DOI:10.1039/jr9300001202

Reference yield:

1-nitro-2-phenoxy-benzene (2216-12-8) → 4-bromo-2-(4-bromo-phenoxy)-aniline (873980-35-9)

Guidance literature:

Multi-step reaction with 5 steps

1: tetrachloromethane; bromine / 100 °C

3: acetic acid

4: acetic acid; sodium acetate; bromine

5: aq.-ethanolic hydrochloric acid

With hydrogenchloride; tetrachloromethane; bromine; sodium acetate; acetic acid;

DOI:10.1039/jr9300001202

Reference yield:

2,4-dibromonitrobenzene (51686-78-3) → 4-bromo-2-(4-bromo-phenoxy)-aniline (873980-35-9)

Guidance literature:

Multi-step reaction with 4 steps

1: phenol; copper-powder / 150 °C

2: glacial acetic acid; bromine

3: tin (II)-chloride; hydrogen chloride; diethyl ether / Umsetzung des Reaktionsprodukts mit Acetanhydrid

4: aq.-ethanolic hydrochloric acid

With hydrogenchloride; diethyl ether; bromine; copper; acetic acid; tin(ll) chloride; phenol;

DOI:10.1039/jr9300001202

upstream raw materials:

acetic acid-[4-bromo-2-(4-bromo-phenoxy)-anilide]

1-nitro-2-phenoxy-benzene

2,4-dibromonitrobenzene

1-(2-nitrophenoxy)-4-bromobenzene

Downstream raw materials:

2,8-dibromodibenzofuran