Technology Process of Thiopyrylium,
1-[3-[4-(1,1-dimethylethyl)phenyl]-2-methylpropyl]hexahydro-, chloride
There total 5 articles about Thiopyrylium,
1-[3-[4-(1,1-dimethylethyl)phenyl]-2-methylpropyl]hexahydro-, chloride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
thionyl chloride;
In
chloroform;
1.) RT, 0.5 h, 2.) 50 deg C, 0.25 h;
DOI:10.1071/CH9920457
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 66 percent / CH3ONa / methanol / 1.25 h / Heating
2: 98 percent / LiAlH4 / tetrahydrofuran / 1.25 h / Heating
3: SOCl2 / CHCl3 / 1.) RT, 0.5 h, 2.) 50 deg C, 0.25 h
With
lithium aluminium tetrahydride; thionyl chloride; sodium methylate;
In
tetrahydrofuran; methanol; chloroform;
DOI:10.1071/CH9920457
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) thiourea, 2.) 20percent aq. NaOH / 1.) DMSO, 120 deg C, 48 h, 2.) reflux, 2 h
2: 66 percent / CH3ONa / methanol / 1.25 h / Heating
3: 98 percent / LiAlH4 / tetrahydrofuran / 1.25 h / Heating
4: SOCl2 / CHCl3 / 1.) RT, 0.5 h, 2.) 50 deg C, 0.25 h
With
sodium hydroxide; lithium aluminium tetrahydride; thionyl chloride; sodium methylate; thiourea;
In
tetrahydrofuran; methanol; chloroform;
DOI:10.1071/CH9920457
