3,5-Pyridinedicarboxylic acid, 2-[(2-azidoethoxy)methyl]-4-(2,3-dichlorophenyl)-1,4-dihydro-6-methyl-, 5-methyl 3-[2-(phenylmethoxy)ethyl] ester

Base Information

• Chemical Name: 3,5-Pyridinedicarboxylic acid, 2-[(2-azidoethoxy)methyl]-4-(2,3-dichlorophenyl)-1,4-dihydro-6-methyl-, 5-methyl 3-[2-(phenylmethoxy)ethyl] ester
• CAS No.: 140171-62-6
• Molecular Formula: C27H28Cl2N4O6
• Molecular Weight: 575.449

Synonyms:

Chemical Property of 3,5-Pyridinedicarboxylic acid, 2-[(2-azidoethoxy)methyl]-4-(2,3-dichlorophenyl)-1,4-dihydro-6-methyl-, 5-methyl 3-[2-(phenylmethoxy)ethyl] ester

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Technology Process of 3,5-Pyridinedicarboxylic acid, 2-[(2-azidoethoxy)methyl]-4-(2,3-dichlorophenyl)-1,4-dihydro-6-methyl-, 5-methyl 3-[2-(phenylmethoxy)ethyl] ester

There total 2 articles about 3,5-Pyridinedicarboxylic acid, 2-[(2-azidoethoxy)methyl]-4-(2,3-dichlorophenyl)-1,4-dihydro-6-methyl-, 5-methyl 3-[2-(phenylmethoxy)ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-azidoethoxymethyl)-3-carboxy-4-(2,3-dichlorophenyl)-5-(methoxycarbonyl)-6-methyl-1,4-dihydropyridine → 2-(2-Azido-ethoxymethyl)-4-(2,3-dichloro-phenyl)-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-benzyloxy-ethyl) ester 5-methyl ester (140171-62-6)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.5 h / Ambient temperature

2: tetrahydrofuran / Ambient temperature

In tetrahydrofuran; dichloromethane;

DOI:10.1016/0223-5234(91)90132-7

Reference yield:

2-Benzyloxyethanol (622-08-2,1201808-31-2) + 6-(2-Azido-ethoxymethyl)-4-(2,3-dichloro-phenyl)-5-(imidazole-1-carbonyl)-2-methyl-1,4-dihydro-pyridine-3-carboxylic acid methyl ester → 2-(2-Azido-ethoxymethyl)-4-(2,3-dichloro-phenyl)-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-benzyloxy-ethyl) ester 5-methyl ester (140171-62-6)

Guidance literature:

In tetrahydrofuran; Ambient temperature;

DOI:10.1016/0223-5234(91)90132-7

Reference yield: 26.0%

2-(2-Azido-ethoxymethyl)-4-(2,3-dichloro-phenyl)-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-benzyloxy-ethyl) ester 5-methyl ester (140171-62-6) → 2-(2-Amino-ethoxymethyl)-4-(2,3-dichloro-phenyl)-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-benzyloxy-ethyl) ester 5-methyl ester (140171-77-3)

Guidance literature:

With hydrogen; Lindlar's catalyst; In ethanol; Ambient temperature;

DOI:10.1016/0223-5234(91)90132-7

upstream raw materials:

2-Benzyloxyethanol

Downstream raw materials:

2-(2-Amino-ethoxymethyl)-4-(2,3-dichloro-phenyl)-6-methyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-(2-benzyloxy-ethyl) ester 5-methyl ester

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