C₁₇H₁₄O

Base Information

• Chemical Name: C₁₇H₁₄O
• CAS No.: 111373-42-3
• Molecular Formula: C₁₇H₁₄O
• Molecular Weight: 234.298
• Mol file: 111373-42-3.mol

Synonyms:

Chemical Property of C₁₇H₁₄O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₄O

There total 4 articles about C₁₇H₁₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9,10-dihydro-9,10-ethanoanthracene-11-methanol (6624-25-5,111389-89-0) → C17H14O (7673-68-9,111373-42-3)

Guidance literature:

With oxalyl dichloride; triethylamine; In dichloromethane; dimethyl sulfoxide; from -78 deg C to room temperature;

DOI:10.1016/S0040-4039(00)95681-8

Reference yield:

anthracene (120-12-7) → C17H14O (7673-68-9,111373-42-3)

Guidance literature:

Multi-step reaction with 4 steps

1: TiCl₄ / CH₂Cl₂ / 25 °C

2: 97 percent / LiOH / tetrahydrofuran; H₂O / Ambient temperature

3: 99 percent / LAH

4: (COCl)2, NEt₃ / CH₂Cl₂; dimethylsulfoxide / from -78 deg C to room temperature

With lithium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; titanium tetrachloride; triethylamine; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;

DOI:10.1016/S0040-4039(00)95681-8

Reference yield:

C17H14O2 (111373-41-2) → C17H14O (7673-68-9,111373-42-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 99 percent / LAH

2: (COCl)2, NEt₃ / CH₂Cl₂; dimethylsulfoxide / from -78 deg C to room temperature

With lithium aluminium tetrahydride; oxalyl dichloride; triethylamine; In dichloromethane; dimethyl sulfoxide;

DOI:10.1016/S0040-4039(00)95681-8

upstream raw materials:

9,10-dihydro-9,10-ethanoanthracene-11-methanol

anthracene

C₁₇H₁₄O₂

C₂₃H₂₂O₄

Downstream raw materials:

9,10-dihydro-9,10-ethanoanthracene-11-methanol