1,8-Naphthalenediol, decahydro-, (1alpha,4abeta,8alpha,8aalpha)-

Base Information

Chemical Name:1,8-Naphthalenediol, decahydro-, (1alpha,4abeta,8alpha,8aalpha)-
CAS No.:135080-42-1
Molecular Formula:C₁₀H₁₈O₂
Molecular Weight:170.252
Hs Code.:
DSSTox Substance ID:DTXSID001233719

Synonyms:DTXSID001233719;135080-42-1

Suppliers and Price of 1,8-Naphthalenediol, decahydro-, (1alpha,4abeta,8alpha,8aalpha)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,8-Naphthalenediol, decahydro-, (1alpha,4abeta,8alpha,8aalpha)-

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:170.130679813
Heavy Atom Count:12
Complexity:142

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC2CCCC(C2C(C1)O)O
Isomeric SMILES:C1C[C@H](C2[C@H](CCCC2C1)O)O

Technology Process of 1,8-Naphthalenediol, decahydro-, (1alpha,4abeta,8alpha,8aalpha)-

There total 11 articles about 1,8-Naphthalenediol, decahydro-, (1alpha,4abeta,8alpha,8aalpha)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 135080-45-4
(+/-)-4-(Cyclohex-2-enyl)butan-1-ol

: 91241-20-2,95295-54-8,135080-42-1,135080-49-8
(1R,8R)-Decahydro-naphthalene-1,8-diol

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / CH₂Cl₂ / 4 °C

2: sodium iodide / acetone / 22 °C

3: 59 percent / AgNO₂ / diethyl ether / 1.) 0 deg C, 24 h, 2.) 22 deg C, 48 h

4: phenyl isocyanate; NEt₃ / benzene / 15 h / Heating

5: H₂, acetic acid / Raney-nickel / methanol; H₂O / 3 h / 22 °C

6: NaBH₄ / methanol / 1.) 0 deg C, 30 min, 2.) 22 deg C, 2 h

With sodium tetrahydroborate; silver(I) nitrite; hydrogen; phenyl isocyanate; acetic acid; triethylamine; sodium iodide; nickel; In methanol; diethyl ether; dichloromethane; water; acetone; benzene;

Reference yield:

: 3-(4-Iodo-butyl)-cyclohexene

: 91241-20-2,95295-54-8,135080-42-1,135080-49-8
(1R,8R)-Decahydro-naphthalene-1,8-diol

Guidance literature:: Multi-step reaction with 4 steps

1: 59 percent / AgNO₂ / diethyl ether / 1.) 0 deg C, 24 h, 2.) 22 deg C, 48 h

2: phenyl isocyanate; NEt₃ / benzene / 15 h / Heating

3: H₂, acetic acid / Raney-nickel / methanol; H₂O / 3 h / 22 °C

4: NaBH₄ / methanol / 1.) 0 deg C, 30 min, 2.) 22 deg C, 2 h

With sodium tetrahydroborate; silver(I) nitrite; hydrogen; phenyl isocyanate; acetic acid; triethylamine; nickel; In methanol; diethyl ether; water; benzene;

Reference yield:

: 135080-51-2
3-(4,4-Dimethoxy-butyl)-cyclohexene

: 91241-20-2,95295-54-8,135080-42-1,135080-49-8
(1R,8R)-Decahydro-naphthalene-1,8-diol

Guidance literature:: Multi-step reaction with 7 steps

1: 1) p-TsOH, 2) NaBH₄ / 1) acetone, 22 deg C, overnight, 2) MeOH, 1 h

2: 95 percent / CH₂Cl₂ / 4 °C

3: sodium iodide / acetone / 22 °C

4: 59 percent / AgNO₂ / diethyl ether / 1.) 0 deg C, 24 h, 2.) 22 deg C, 48 h

5: phenyl isocyanate; NEt₃ / benzene / 15 h / Heating

6: H₂, acetic acid / Raney-nickel / methanol; H₂O / 3 h / 22 °C

7: NaBH₄ / methanol / 1.) 0 deg C, 30 min, 2.) 22 deg C, 2 h

With sodium tetrahydroborate; silver(I) nitrite; hydrogen; phenyl isocyanate; toluene-4-sulfonic acid; acetic acid; triethylamine; sodium iodide; nickel; In methanol; diethyl ether; dichloromethane; water; acetone; benzene;