1,2,2a,8b-tetramethyl-4H-cyclobuta[c]quinoline-3-thione

Base Information

Chemical Name:1,2,2a,8b-tetramethyl-4H-cyclobuta[c]quinoline-3-thione
CAS No.:81045-15-0
Molecular Formula:C₁₅H₁₇NS
Molecular Weight:243.373
Hs Code.:
NSC Number:366208
DSSTox Substance ID:DTXSID90392123

Synonyms:81045-15-0;NSC366208;1,2,2a,8b-tetramethyl-4H-cyclobuta[c]quinoline-3-thione;DTXSID90392123;NSC-366208

Suppliers and Price of 1,2,2a,8b-tetramethyl-4H-cyclobuta[c]quinoline-3-thione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1,2,2a,8b-tetramethyl-4H-cyclobuta[c]quinoline-3-thione

Chemical Property:

Vapor Pressure:0.00045mmHg at 25°C
XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:243.10817072
Heavy Atom Count:17
Complexity:425

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C2(C1(C3=CC=CC=C3NC2=S)C)C)C

Technology Process of 1,2,2a,8b-tetramethyl-4H-cyclobuta[c]quinoline-3-thione

There total 3 articles about 1,2,2a,8b-tetramethyl-4H-cyclobuta[c]quinoline-3-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 81045-14-9
1,4,5,6-tetramethyl-2-thia-3-(phenylimino)bicyclo<2.2.0>hex-5-ene

: 81045-15-0
4,5-benzo-1,6,7,8-tetramethyl-3-aza-2-thioxobicyclo<4.2.0>oct-7-ene

Guidance literature:: With aluminium trichloride; In dichloromethane; for 72h;
DOI:10.1021/jo00349a017

Reference yield:

: 103-72-0
phenyl isothiocyanate

: 81045-15-0
4,5-benzo-1,6,7,8-tetramethyl-3-aza-2-thioxobicyclo<4.2.0>oct-7-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) AlCl₃ / 1.) CH₂Cl₂, 2.) RT, 10 h

2: 12 percent / AlCl₃ / CH₂Cl₂ / 72 h

With aluminium trichloride; In dichloromethane;
DOI:10.1021/jo00349a017

Reference yield:

: 503-17-3
dimethylacetylene

: 103-72-0
phenyl isothiocyanate

: 81045-15-0
4,5-benzo-1,6,7,8-tetramethyl-3-aza-2-thioxobicyclo<4.2.0>oct-7-ene

: 81045-14-9
1,4,5,6-tetramethyl-2-thia-3-(phenylimino)bicyclo<2.2.0>hex-5-ene

Guidance literature:: With aluminium trichloride; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, 2.) RT, 10 h;
DOI:10.1021/jo00349a017