3-[3,3'''-didodecyl-5'''-[3-(2,3,4,6-tetra-O-acetyl-α-L-mannopyranosyloxy)-1-propyn-1-yl][2,2':5',2'':5'',2'''-quaterthien]-5-yl]-2-propyn-1-yl-α-L-mannopyranose tetraacetate

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Chemical Name:3-[3,3'''-didodecyl-5'''-[3-(2,3,4,6-tetra-O-acetyl-α-L-mannopyranosyloxy)-1-propyn-1-yl][2,2':5',2'':5'',2'''-quaterthien]-5-yl]-2-propyn-1-yl-α-L-mannopyranose tetraacetate
CAS No.:1194524-98-5
Molecular Formula:C₇₄H₉₈O₂₀S₄
Molecular Weight:1435.84
Hs Code.:

3-[3,3'''-didodecyl-5'''-[3-(2,3,4,6-tetra-O-acetyl-α-L-mannopyranosyloxy)-1-propyn-1-yl][2,2':5',2'':5'',2'''-quaterthien]-5-yl]-2-propyn-1-yl-α-L-mannopyranose tetraacetate

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Chemical Property of 3-[3,3'''-didodecyl-5'''-[3-(2,3,4,6-tetra-O-acetyl-α-L-mannopyranosyloxy)-1-propyn-1-yl][2,2':5',2'':5'',2'''-quaterthien]-5-yl]-2-propyn-1-yl-α-L-mannopyranose tetraacetate

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Technology Process of 3-[3,3'''-didodecyl-5'''-[3-(2,3,4,6-tetra-O-acetyl-α-L-mannopyranosyloxy)-1-propyn-1-yl][2,2':5',2'':5'',2'''-quaterthien]-5-yl]-2-propyn-1-yl-α-L-mannopyranose tetraacetate

There total 1 articles about 3-[3,3'''-didodecyl-5'''-[3-(2,3,4,6-tetra-O-acetyl-α-L-mannopyranosyloxy)-1-propyn-1-yl][2,2':5',2'':5'',2'''-quaterthien]-5-yl]-2-propyn-1-yl-α-L-mannopyranose tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1194524-95-2
2-propynyl-2,3,4,6-tetra-O-acetyl-α-L-(-)-mannopyranoside

: 874108-24-4,827343-06-6
5,5'''-diiodo-3,3'''-didodecyl-[2,2';5',2'';5'',2''']quaterthiophene

: 1194524-98-5,827343-06-6
3-[3,3'''-didodecyl-5'''-[3-(2,3,4,6-tetra-O-acetyl-α-L-mannopyranosyloxy)-1-propyn-1-yl][2,2':5',2'':5'',2'''-quaterthien]-5-yl]-2-propyn-1-yl-α-L-mannopyranose tetraacetate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol9022694

Reference yield: 97.0%

: 1194524-98-5,827343-06-6
3-[3,3'''-didodecyl-5'''-[3-(2,3,4,6-tetra-O-acetyl-α-L-mannopyranosyloxy)-1-propyn-1-yl][2,2':5',2'':5'',2'''-quaterthien]-5-yl]-2-propyn-1-yl-α-L-mannopyranose tetraacetate

: 1194525-00-2,827343-06-6
3-[3,3'''-didodecyl-5'''-[3-(α-L-mannopyranosyloxy)-1-propyn-1-yl][2,2':5',2'':5'',2'''-quaterthien]-5-yl]-2-propyn-1-yl-α-L-mannopyranoside

Guidance literature:: 3-[3,3'''-didodecyl-5'''-[3-(2,3,4,6-tetra-O-acetyl-α-L-mannopyranosyloxy)-1-propyn-1-yl][2,2':5',2'':5'',2'''-quaterthien]-5-yl]-2-propyn-1-yl-α-L-mannopyranose tetraacetate; With methanol; sodium methylate; In tetrahydrofuran; for 1h; Inert atmosphere;

In tetrahydrofuran; methanol; Inert atmosphere;
DOI:10.1021/ol9022694