D-xylo-D-allo-Dodeconic acid, 3,7:6,10-dianhydro-8,9-O-cyclohexylidene-2,4,5-trideoxy-, methyl ester

Base Information

Chemical Name:D-xylo-D-allo-Dodeconic acid, 3,7:6,10-dianhydro-8,9-O-cyclohexylidene-2,4,5-trideoxy-, methyl ester
CAS No.:871360-12-2
Molecular Formula:C₁₉H₃₀O₈
Molecular Weight:386.442
Hs Code.:

Synonyms:

Suppliers and Price of D-xylo-D-allo-Dodeconic acid, 3,7:6,10-dianhydro-8,9-O-cyclohexylidene-2,4,5-trideoxy-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 4 raw suppliers

Chemical Property of D-xylo-D-allo-Dodeconic acid, 3,7:6,10-dianhydro-8,9-O-cyclohexylidene-2,4,5-trideoxy-, methyl ester

Chemical Property:

Boiling Point:557.0±45.0 °C(Predicted)
PKA:13.35±0.20(Predicted)
Density:1.31±0.1 g/cm3(Predicted)
Storage Temp.:Inert atmosphere,Store in freezer, under -20°C

Purity/Quality:: 95-424%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of D-xylo-D-allo-Dodeconic acid, 3,7:6,10-dianhydro-8,9-O-cyclohexylidene-2,4,5-trideoxy-, methyl ester

There total 9 articles about D-xylo-D-allo-Dodeconic acid, 3,7:6,10-dianhydro-8,9-O-cyclohexylidene-2,4,5-trideoxy-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 871360-11-1
C₂₅H₃₆O₁₁

: 871360-12-2
methyl 2-((3aR,4S,5aS,8R,9aS,9bS)-4-((R)-1,2-dihydroxyethyl)octahydrospiro[[1,3]dioxolo[4,5-d]pyrano[3,2-b]pyran-2,1'-cyclohexan]-8-yl)acetate

Guidance literature:: With N-benzyl-trimethylammonium hydroxide; In tetrahydrofuran; acetic acid methyl ester; at 17 - 23 ℃; for 1.53333h; Product distribution / selectivity;

Reference yield: 62.0%

: C₂₃H₃₄O₁₀

: 871360-12-2
methyl 2-((3aR,4S,5aS,8R,9aS,9bS)-4-((R)-1,2-dihydroxyethyl)octahydrospiro[[1,3]dioxolo[4,5-d]pyrano[3,2-b]pyran-2,1'-cyclohexan]-8-yl)acetate

Guidance literature:: With sodium methylate; In methanol; tert-butyl methyl ether; at 15 ℃;
DOI:10.1055/s-0032-1317919

Reference yield:

: 871360-09-7
C₁₉H₃₀O₇

: 871360-12-2
methyl 2-((3aR,4S,5aS,8R,9aS,9bS)-4-((R)-1,2-dihydroxyethyl)octahydrospiro[[1,3]dioxolo[4,5-d]pyrano[3,2-b]pyran-2,1'-cyclohexan]-8-yl)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: zinc(II) chloride; acetic acid / 30 °C

2: boron trifluoride diethyl etherate / acetonitrile / 15 °C

3: sodium methylate / methanol; tert-butyl methyl ether / 15 °C

With boron trifluoride diethyl etherate; sodium methylate; acetic acid; zinc(II) chloride; In methanol; tert-butyl methyl ether; acetonitrile;
DOI:10.1055/s-0032-1317919