(+/-)-10-METHYLOCTADECANOIC ACID

Base Information

Chemical Name:(+/-)-10-METHYLOCTADECANOIC ACID
CAS No.:80508-15-2
Molecular Formula:C₁₉H₃₈O₂
Molecular Weight:298.51
Hs Code.:
Mol file:80508-15-2.mol

Synonyms:

Suppliers and Price of (+/-)-10-METHYLOCTADECANOIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
10-METHYLOCTADECANOIC ACID 95.00%
1MG
$ 647.61

Total 3 raw suppliers

Chemical Property of (+/-)-10-METHYLOCTADECANOIC ACID

Chemical Property:

Storage Temp.:−20°C

Purity/Quality:: 10-METHYLOCTADECANOIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-10-METHYLOCTADECANOIC ACID

There total 58 articles about (+/-)-10-METHYLOCTADECANOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 2490-04-2
(R,S)-10-methyloctadecanol

: 542-47-2,80508-15-2
10-Methyl-octadecanoic acid

Guidance literature:: With dipyridinium dichromate; 4 A molecular sieve; In N,N-dimethyl-formamide; for 120h; Ambient temperature;
DOI:10.1016/0009-3084(94)90067-1

Reference yield:

: 629-11-8
1,6-hexanediol

: 542-47-2,80508-15-2
10-Methyl-octadecanoic acid

Guidance literature:: Multi-step reaction with 8 steps

1: 48 percent / iron (III) sulphate on silica gel / hexane / 1.42 h / 45 °C

2: 84 percent / pyridine / CH₂Cl₂ / 16 h / Ambient temperature

3: 46 percent / I₂, 1,2-bis(diphenylphosphino)ethane / CH₂Cl₂ / 4 h / Ambient temperature

4: 34 percent / dimethylsulfoxide / 2 h / Ambient temperature

5: 79 percent / trifluoroacetic acid, H₂O / CH₂Cl₂

6: 1.) n-BuLi, 2.) HMPA / 1.) THF, hexane, 0 deg C, 10 min, 2.) THF, hexane, 0 deg C, 1.5 h

7: 88 percent / H₂ / 10percent Pd/C / diethyl ether / 16 h

8: 44 percent / molecular sieves 4 A, pyridinum dichromate / dimethylformamide / 120 h / Ambient temperature

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dipyridinium dichromate; n-butyllithium; 4 A molecular sieve; water; hydrogen; iodine; trifluoroacetic acid; 1,2-bis-(diphenylphosphino)ethane; iron(III) sulfate; palladium on activated charcoal; In diethyl ether; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/0009-3084(94)90067-1

Reference yield:

: 18675-24-6
2-methyldecan-1-ol

: 542-47-2,80508-15-2
10-Methyl-octadecanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 60 percent / I₂, chlorodiphenylphosphine, imidazole / toluene / 3 h / 70 °C

2: 1.) n-BuLi, 2.) HMPA / 1.) THF, hexane, from -78 deg C to RT, 1 h, 2.) THF, hexane, form -78 deg C to RT, 4 h

3: 68 percent / methanolic para-toluenesulfonic acid / toluene / 144 h

4: 88 percent / H₂ / 10percent Pd/C / diethyl ether / 16 h

5: 44 percent / molecular sieves 4 A, pyridinum dichromate / dimethylformamide / 120 h / Ambient temperature

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; dipyridinium dichromate; n-butyllithium; 4 A molecular sieve; hydrogen; iodine; toluene-4-sulfonic acid; chloro-diphenylphosphine; palladium on activated charcoal; In diethyl ether; N,N-dimethyl-formamide; toluene;
DOI:10.1016/0009-3084(94)90067-1