6-(1,3-benzodioxol-5-yl)-7,8-dihydro-6H-benzo[f][1,3]benzodioxol-5-one

Base Information

Chemical Name:6-(1,3-benzodioxol-5-yl)-7,8-dihydro-6H-benzo[f][1,3]benzodioxol-5-one
CAS No.:88775-69-3
Molecular Formula:C₁₈H₁₄O₅
Molecular Weight:310.306
Hs Code.:
NSC Number:166714
DSSTox Substance ID:DTXSID80304654
ChEMBL ID:CHEMBL1880554

Synonyms:MLS003106619;88775-69-3;NSC166714;CHEMBL1880554;DTXSID80304654;NSC-166714;SMR001821512

Suppliers and Price of 6-(1,3-benzodioxol-5-yl)-7,8-dihydro-6H-benzo[f][1,3]benzodioxol-5-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 6-(1,3-benzodioxol-5-yl)-7,8-dihydro-6H-benzo[f][1,3]benzodioxol-5-one

Chemical Property:

Vapor Pressure:1.86E-10mmHg at 25°C
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:1
Exact Mass:310.08412354
Heavy Atom Count:23
Complexity:480

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC2=CC3=C(C=C2C(=O)C1C4=CC5=C(C=C4)OCO5)OCO3

Technology Process of 6-(1,3-benzodioxol-5-yl)-7,8-dihydro-6H-benzo[f][1,3]benzodioxol-5-one

There total 6 articles about 6-(1,3-benzodioxol-5-yl)-7,8-dihydro-6H-benzo[f][1,3]benzodioxol-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88755-23-1
2,4-bis(3,4-methylenedioxyphenyl)-4-oxobutyronitrile

: 88775-69-3
6,7-methylenedioxy-2-(3,4-methylenedioxyphenyl)-3,4-dihydronaphthalen-1(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 0.19 g / NaOH / aq. ethanol / 10 h / Heating

2: 3.16 g / hydrogen / PdCl₂ aq./Norit / acetic acid / Ambient temperature

3: 3.86 g / POCl₃ / CHCl₃ / 4.2 h / Heating

With sodium hydroxide; hydrogen; trichlorophosphate; pyrographite; palladium dichloride; In ethanol; chloroform; acetic acid;
DOI:10.1248/cpb.31.3039

Reference yield:

: 88755-27-5
2,4-bis(3,4-methylenedioxyphenyl)-4-oxobutyramide

: 88775-69-3
6,7-methylenedioxy-2-(3,4-methylenedioxyphenyl)-3,4-dihydronaphthalen-1(2H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 0.87 g / hydrogen / PdCl₂ aq./Norit / acetic acid / Ambient temperature

2: 8.16 g / 33percent KOH aq. / ethanol / 11 h / Heating

3: 3.86 g / POCl₃ / CHCl₃ / 4.2 h / Heating

With potassium hydroxide; hydrogen; trichlorophosphate; pyrographite; palladium dichloride; In ethanol; chloroform; acetic acid;
DOI:10.1248/cpb.31.3039

Reference yield:

: 88755-39-9
2,4-bis(3,4-methylenedioxyphenyl)-4-oxobutyric acid

: 88775-69-3
6,7-methylenedioxy-2-(3,4-methylenedioxyphenyl)-3,4-dihydronaphthalen-1(2H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 3.16 g / hydrogen / PdCl₂ aq./Norit / acetic acid / Ambient temperature

2: 3.86 g / POCl₃ / CHCl₃ / 4.2 h / Heating

With hydrogen; trichlorophosphate; pyrographite; palladium dichloride; In chloroform; acetic acid;
DOI:10.1248/cpb.31.3039