pentyl 3,3-dimethylbutyrate

Base Information

Chemical Name:pentyl 3,3-dimethylbutyrate
CAS No.:101186-00-9
Molecular Formula:C₁₁H₂₂O₂
Molecular Weight:186.294
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentyl 3,3-dimethylbutyrate

Chemical Property:

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Technology Process of pentyl 3,3-dimethylbutyrate

There total 3 articles about pentyl 3,3-dimethylbutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 4-iodopentyl 3,3-dimethylbutyrate

: 101186-00-9
pentyl 3,3-dimethylbutyrate

Guidance literature:: With [1,3-bis(2,6-di-iso-propylphenyl)imidazol-2-ylidene]copper(I) tert-butoxide; diphenylsilane; 2-tert-butylphenol potassium salt; In 1,4-dioxane; at 25 ℃; for 24h; chemoselective reaction; Inert atmosphere; Glovebox;
DOI:10.1016/j.tet.2014.04.004

Reference yield:

: 71-41-0
pentan-1-ol

: 1070-83-3
tert-Butylacetic acid

: 101186-00-9
pentyl 3,3-dimethylbutyrate

Guidance literature:: With sulfuric acid; at 40 ℃; for 2h; Yield given;
DOI:10.1055/s-1985-31243

Reference yield:

: C₁₁H₂₂O₃

: 101186-00-9
pentyl 3,3-dimethylbutyrate

Guidance literature:: Multi-step reaction with 2 steps

1: iodine; triphenylphosphine; 1H-imidazole / benzene / Inert atmosphere; Reflux

2: diphenylsilane; [1,3-bis(2,6-di-iso-propylphenyl)imidazol-2-ylidene]copper(I) tert-butoxide; 2-tert-butylphenol potassium salt / 1,4-dioxane / 24 h / 25 °C / Inert atmosphere

With 1H-imidazole; [1,3-bis(2,6-di-iso-propylphenyl)imidazol-2-ylidene]copper(I) tert-butoxide; diphenylsilane; iodine; triphenylphosphine; 2-tert-butylphenol potassium salt; In 1,4-dioxane; benzene;
DOI:10.1002/anie.201307697