6β-hydroxyloganin

Base Information

Chemical Name:6β-hydroxyloganin
CAS No.:115075-53-1
Molecular Formula:C₁₇H₂₆O₁₁
Molecular Weight:406.387
Hs Code.:

Synonyms:

Suppliers and Price of 6β-hydroxyloganin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 6β-hydroxyloganin

Chemical Property:

Purity/Quality:: ≥95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6β-hydroxyloganin

There total 3 articles about 6β-hydroxyloganin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7-O-trans-cinnamoyl 6β-hydroxyloganin

: 115075-53-1,125410-24-4,125410-28-8,84395-22-2
6β-hydroxyloganin

Guidance literature:: With hydroxylamine sulfate; triethylamine; In tetrahydrofuran; ethanol; water; at 20 - 110 ℃; for 6h;
DOI:10.1016/j.phymed.2013.08.023

Reference yield:

: 125323-69-5
6β-hydroxyloganin tetraacetate

: 115075-53-1,125410-24-4,125410-28-8,84395-22-2
6β-hydroxyloganin

Guidance literature:: With sodium methylate; In methanol; for 0.5h;
DOI:10.1016/0031-9422(89)80263-8

Reference yield:

: (1S,4aS,6R,7R,7aS)-7-Methyl-6-(toluene-4-sulfonyloxy)-1-((2S,3R,4S,5R,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-1,4a,5,6,7,7a-hexahydro-cyclopenta[c]pyran-4-carboxylic acid methyl ester

: 115075-53-1,125410-24-4,125410-28-8,84395-22-2
6β-hydroxyloganin

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) DBU; 2.) OsO₄ / 1.) THF, reflux, 67 h; 2.) Et₂O, pyridine, 3 min

2: 31.2 mg / methanolic NaOMe / methanol / 0.5 h

With osmium(VIII) oxide; sodium methylate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol;
DOI:10.1016/0031-9422(89)80263-8