3,4-dihydro-3,4-dihydroxybenzacridine

Base Information

Chemical Name:3,4-dihydro-3,4-dihydroxybenzacridine
CAS No.:78167-93-8
Molecular Formula:C₁₇H₁₃NO₂
Molecular Weight:263.296
Hs Code.:

3,4-dihydro-3,4-dihydroxybenz<c>acridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-dihydro-3,4-dihydroxybenzacridine

Chemical Property:

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Technology Process of 3,4-dihydro-3,4-dihydroxybenzacridine

There total 16 articles about 3,4-dihydro-3,4-dihydroxybenzacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 78167-92-7
(+/-)-trans-3,4-Diacetoxy-3,4-dihydrobenzacridine

: 78167-93-8,77305-76-1
3,4-dihydro-3,4-dihydroxybenzacridine

Guidance literature:: With ammonia; In tetrahydrofuran; methanol; for 2h; Ambient temperature;
DOI:10.1021/jo00331a019

Reference yield: 19.7%

: 111351-49-6
3,4-dioxo-3,4-dihydrobenzacridine

: 78167-93-8,77305-76-1
3,4-dihydro-3,4-dihydroxybenzacridine

: 111351-47-4
3-hydroxybenzacridine

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 48h; Yields of byproduct given; Ambient temperature;
DOI:10.1021/jo00236a049

Reference yield:

: 72019-93-3
3-methoxy-5,6-dihydronaphtho<1,2-b>quinoline

: 78167-93-8,77305-76-1
3,4-dihydro-3,4-dihydroxybenzacridine

Guidance literature:: Multi-step reaction with 4 steps

1: 94.1 percent / p-cymene / 10percent Pd-C / 2 h / Heating

2: 89.9 percent / 48percent HBr / 2.25 h / Heating

3: 85 percent / Fremy's salt, KH₂PO₄ buffer / H₂O; methanol; tetrahydrofuran / 2 h / 0 - 15 °C

4: 19.7 percent / NaBH₄ / ethanol / 48 h / Ambient temperature

With sodium tetrahydroborate; KH₂PO₄ buffer; potassiuim nitrosodisulfonate; 4-methylisopropylbenzene; hydrogen bromide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; water;
DOI:10.1021/jo00236a049