Technology Process of 3,4-dihydro-3,4-dihydroxybenzacridine
There total 16 articles about 3,4-dihydro-3,4-dihydroxybenzacridine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonia;
In
tetrahydrofuran; methanol;
for 2h;
Ambient temperature;
DOI:10.1021/jo00331a019
- Guidance literature:
-
With
sodium tetrahydroborate;
In
ethanol;
for 48h;
Yields of byproduct given;
Ambient temperature;
DOI:10.1021/jo00236a049
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 94.1 percent / p-cymene / 10percent Pd-C / 2 h / Heating
2: 89.9 percent / 48percent HBr / 2.25 h / Heating
3: 85 percent / Fremy's salt, KH2PO4 buffer / H2O; methanol; tetrahydrofuran / 2 h / 0 - 15 °C
4: 19.7 percent / NaBH4 / ethanol / 48 h / Ambient temperature
With
sodium tetrahydroborate; KH2PO4 buffer; potassiuim nitrosodisulfonate; 4-methylisopropylbenzene; hydrogen bromide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethanol; water;
DOI:10.1021/jo00236a049
