(22S,23S)-2α,3α,22,23-tetrahydroxy-B-homo-7-oxa-5α-cholestan-6-on

Base Information

Chemical Name:(22S,23S)-2α,3α,22,23-tetrahydroxy-B-homo-7-oxa-5α-cholestan-6-on
CAS No.:86695-23-0
Molecular Formula:C₂₇H₄₆O₆
Molecular Weight:466.659
Hs Code.:

Synonyms:

Suppliers and Price of (22S,23S)-2α,3α,22,23-tetrahydroxy-B-homo-7-oxa-5α-cholestan-6-on

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (22S,23S)-2α,3α,22,23-tetrahydroxy-B-homo-7-oxa-5α-cholestan-6-on

Chemical Property:

Purity/Quality:

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Technology Process of (22S,23S)-2α,3α,22,23-tetrahydroxy-B-homo-7-oxa-5α-cholestan-6-on

There total 8 articles about (22S,23S)-2α,3α,22,23-tetrahydroxy-B-homo-7-oxa-5α-cholestan-6-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 83456-52-4,83462-93-5
(22S,23S)-2α,3α,22,23-tetraacetoxy-B-homo-7-oxa-5α-cholestan-6-on

: 77736-43-7,78780-31-1,86695-23-0,86695-24-1
(22S,23S)-2α,3α,22,23-tetrahydroxy-B-homo-7-oxa-5α-cholestan-6-on

Guidance literature:: With potassium hydroxide; In methanol; Heating;

Reference yield:

: 86400-79-5
C₂₅H₄₀O₅

: 77736-43-7,78780-31-1,86695-23-0,86695-24-1
(22R,23R)-28-norbrassinolide

Guidance literature:: Multi-step reaction with 6 steps

1: 75 percent / pyridinium chlorochromate, sodium acetate

3: 100 percent / red mercuric oxide, boron trifluoride etherate / tetrahydrofuran; H₂O

4: 73 percent / tetrahydrofuran / -78 °C

6: 1.) 5percent KOH, 2.) 6 M HCl / 1.) MeOH, reflux

With hydrogenchloride; potassium hydroxide; boron trifluoride diethyl etherate; sodium acetate; pyridinium chlorochromate; mercury(II) oxide; In tetrahydrofuran; water;
DOI:10.1016/S0040-4039(00)81524-5

Reference yield:

: 86400-80-8
C₂₅H₃₈O₅

: 77736-43-7,78780-31-1,86695-23-0,86695-24-1
(22R,23R)-28-norbrassinolide

Guidance literature:: Multi-step reaction with 5 steps

2: 100 percent / red mercuric oxide, boron trifluoride etherate / tetrahydrofuran; H₂O

3: 73 percent / tetrahydrofuran / -78 °C

5: 1.) 5percent KOH, 2.) 6 M HCl / 1.) MeOH, reflux

With hydrogenchloride; potassium hydroxide; boron trifluoride diethyl etherate; mercury(II) oxide; In tetrahydrofuran; water;
DOI:10.1016/S0040-4039(00)81524-5