benzo[e]pyren-1-ol

Base Information

Chemical Name:benzo[e]pyren-1-ol
CAS No.:77508-25-9
Molecular Formula:C₂₀H₁₂O
Molecular Weight:268.315
Hs Code.:

Synonyms:

Suppliers and Price of benzo[e]pyren-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzo[e]pyren-1-ol

Chemical Property:

Vapor Pressure:9.85E-12mmHg at 25°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of benzo[e]pyren-1-ol

There total 7 articles about benzo[e]pyren-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 77508-24-8
1-Methoxy-benzopyrene

: 77508-25-9
1-Hydroxybenzopyrene

Guidance literature:: With sodium hydride; ethanethiol; In N,N-dimethyl-formamide; for 3h; Heating;
DOI:10.1021/jo00327a010

Reference yield:

: 68151-09-7
9-Hydroxy-1,2,3,6,7,8,9,10,11,12-decahydrobenzopyrene

: 77508-25-9
1-Hydroxybenzopyrene

Guidance literature:: Multi-step reaction with 7 steps

1: 86 percent / 10percent Pd/C / 2 h / 300 - 320 °C

2: 78 percent / Br₂ / chlorobenzene / 0.25 h / Ambient temperature

3: 91 percent / Cl₂ / various solvent(s) / 0.33 h / Ambient temperature

4: 95 percent / n-Butyllithium/hexane / diethyl ether / 0.5 h / Heating

5: hexamethylphosphoric acid triamide / 20 h / 100 °C

6: 66 percent / n-Butyllithium / diethyl ether / 0.5 h / Heating

7: 99 percent / Ethanethiol, NaH / dimethylformamide / 3 h / Heating

With n-butyllithium; hexane; bromine; chlorine; sodium hydride; ethanethiol; palladium on activated charcoal; In N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1021/jo00327a010

Reference yield:

: 192-97-2
benzo[e]pyrene

: 77508-25-9
1-Hydroxybenzopyrene

Guidance literature:: Multi-step reaction with 6 steps

1: 78 percent / Br₂ / chlorobenzene / 0.25 h / Ambient temperature

2: 91 percent / Cl₂ / various solvent(s) / 0.33 h / Ambient temperature

3: 95 percent / n-Butyllithium/hexane / diethyl ether / 0.5 h / Heating

4: hexamethylphosphoric acid triamide / 20 h / 100 °C

5: 66 percent / n-Butyllithium / diethyl ether / 0.5 h / Heating

6: 99 percent / Ethanethiol, NaH / dimethylformamide / 3 h / Heating

With n-butyllithium; hexane; bromine; chlorine; sodium hydride; ethanethiol; In N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; N,N-dimethyl-formamide; chlorobenzene;
DOI:10.1021/jo00327a010