Welcome to LookChem.com Sign In|Join Free
  • or

Encyclopedia

11-(3-dimethylaminopropyl)-11H-dibenzo-1,4-dithiepin

Base Information Edit
  • Chemical Name:11-(3-dimethylaminopropyl)-11H-dibenzo-1,4-dithiepin
  • CAS No.:81890-72-4
  • Molecular Formula:C18H21NS2
  • Molecular Weight:315.503
  • Hs Code.:
  • Mol file:81890-72-4.mol
11-(3-dimethylaminopropyl)-11H-dibenzo<b,e>-1,4-dithiepin

Synonyms:

Suppliers and Price of 11-(3-dimethylaminopropyl)-11H-dibenzo-1,4-dithiepin
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 0 raw suppliers
Chemical Property of 11-(3-dimethylaminopropyl)-11H-dibenzo-1,4-dithiepin Edit
Chemical Property:
Purity/Quality:
Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:
Useful:
Technology Process of 11-(3-dimethylaminopropyl)-11H-dibenzo-1,4-dithiepin

There total 9 articles about 11-(3-dimethylaminopropyl)-11H-dibenzo-1,4-dithiepin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 4 steps
1: KOH / ethanol / 6 h / Heating
2: 60 percent / triphenylphosphine, H2O / dioxane / 1 h / 40 °C
3: 17 percent / K2CO3, Cu / dimethylformamide / 6 h / Heating
4: 1) n-butyllithium / 1) ether/hexane, 30 min
With potassium hydroxide; n-butyllithium; water; copper; potassium carbonate; triphenylphosphine; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1135/cccc19820072
Guidance literature:
Multi-step reaction with 4 steps
1: KOH / ethanol / 6 h / Heating
2: 60 percent / triphenylphosphine, H2O / dioxane / 1 h / 40 °C
3: 17 percent / K2CO3, Cu / dimethylformamide / 6 h / Heating
4: 1) n-butyllithium / 1) ether/hexane, 30 min
With potassium hydroxide; n-butyllithium; water; copper; potassium carbonate; triphenylphosphine; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1135/cccc19820072
Guidance literature:
Multi-step reaction with 5 steps
1: chlorosulfonic acid / CHCl3 / 1) 3 h room temperature 2) 2 h reflux
2: Zn, hydrochloric acid / dioxane / 1.5 h / 80 - 90 °C
3: liquid ammonia, Na / liquid ammonia / 0.67 h
4: 54 percent / K2CO3, Cu / dimethylformamide / 6 h / Heating
5: 1) n-butyllithium / 1) ether/hexane, 30 min
With hydrogenchloride; chlorosulfonic acid; n-butyllithium; ammonia; sodium; copper; potassium carbonate; zinc; In 1,4-dioxane; chloroform; ammonia; N,N-dimethyl-formamide;
DOI:10.1135/cccc19820072
Post RFQ for Price