Beta-Carboline-1-propionic acid, ethyl ester

Base Information

• Chemical Name: Beta-Carboline-1-propionic acid, ethyl ester
• CAS No.: 90686-24-1
• Molecular Formula: C₁₆H₁₆N₂O₂
• Molecular Weight: 268.315
• Mol file: 90686-24-1.mol

Synonyms:

Chemical Property of Beta-Carboline-1-propionic acid, ethyl ester

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Ethylbeta-carboline-1-propionate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Beta-Carboline-1-propionic acid, ethyl ester

There total 7 articles about Beta-Carboline-1-propionic acid, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl-β-carboline-2N-oxide-1-propionate → ethyl-β-carboline-1-propionate (90686-24-1)

Guidance literature:

With iron(II) sulfate; In methanol; for 1h; Heating;

DOI:10.1016/S0031-9422(00)80351-9

Reference yield:

→ ethyl-β-carboline-1-propionate (90686-24-1)

Guidance literature:

With ethanol; platinum; Hydrogenation;

DOI:10.1093/jat/24.7.567

Reference yield:

canthin-6-one (479-43-6) → ethyl-β-carboline-1-propionate (90686-24-1)

Guidance literature:

Multi-step reaction with 3 steps

1: aqueous methanol. NaOH

2: Raney alloy; aq. NaOH solution

3: SOCl₂ / dann Behandeln mit Aethanol

With sodium hydroxide; thionyl chloride; nickel;

DOI:10.1093/jat/24.7.567

upstream raw materials:

β-carboline-1-propionic acid

canthin-6-one

4,5-dihydro-canthin-6-one

3-(9H-β-carbolin-1-yl)-acrylic acid

Downstream raw materials:

β-carboline-1-propionic acid

Refernces