α-methyl glycoside of sibirosamine

Base Information

Chemical Name:α-methyl glycoside of sibirosamine
CAS No.:92840-94-3
Molecular Formula:C₉H₁₉NO₄
Molecular Weight:205.254
Hs Code.:

Synonyms:

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Chemical Property of α-methyl glycoside of sibirosamine

Chemical Property:

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Technology Process of α-methyl glycoside of sibirosamine

There total 7 articles about α-methyl glycoside of sibirosamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92840-91-0
(3aR,4S,7S,7aR)-6,7-Dihydroxy-4-hydroxymethyl-3,7a-dimethyl-tetrahydro-pyrano[3,4-d]oxazol-2-one

: 92840-94-3,781577-46-6
α-methyl glycoside of sibirosamine

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / Dowex 50 (H+) resin / 18 h / Heating

2: 53 percent / triphenylphosphine, diethyl azodicarboxylate, methyl iodide / benzene / 1 h / 23 °C

3: 79 percent / tri-1-butyltin hydride, benzoyl peroxide / benzene / 0.5 h / Heating

4: potassium hydroxide / 1 h / Heating

With potassium hydroxide; Perbenzoic acid; Dowex 50 (H+) resin; tri-n-butyl-tin hydride; triphenylphosphine; diethylazodicarboxylate; methyl iodide; In benzene;
DOI:10.1016/0008-6215(84)85274-X

Reference yield:

: 80462-84-6
3-N-methyl-(methyl 4-deoxy-3-C-methyl-α-D-altropyranosido)-<3,4-d>-1,3-oxazolidin-2-one

: 92840-94-3,781577-46-6
α-methyl glycoside of sibirosamine

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / triphenylphosphine, diethyl azodicarboxylate, methyl iodide / benzene / 1 h / 23 °C

2: 79 percent / tri-1-butyltin hydride, benzoyl peroxide / benzene / 0.5 h / Heating

3: potassium hydroxide / 1 h / Heating

With potassium hydroxide; Perbenzoic acid; tri-n-butyl-tin hydride; triphenylphosphine; diethylazodicarboxylate; methyl iodide; In benzene;
DOI:10.1016/0008-6215(84)85274-X

Reference yield:

: 92900-36-2
methyl-3-N-(1,2,6-tri-O-acetyl-4-deoxy-3-C-methyl-α,β-D-altropyrano)-<3,4-d>-1,3-oxazolidin-2-one

: 92840-94-3,781577-46-6
α-methyl glycoside of sibirosamine

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / sodium methoxide / methanol / 0.75 h / 23 °C

2: 93 percent / Dowex 50 (H+) resin / 18 h / Heating

3: 53 percent / triphenylphosphine, diethyl azodicarboxylate, methyl iodide / benzene / 1 h / 23 °C

4: 79 percent / tri-1-butyltin hydride, benzoyl peroxide / benzene / 0.5 h / Heating

5: potassium hydroxide / 1 h / Heating

With potassium hydroxide; Perbenzoic acid; Dowex 50 (H+) resin; tri-n-butyl-tin hydride; sodium methylate; triphenylphosphine; diethylazodicarboxylate; methyl iodide; In methanol; benzene;
DOI:10.1016/0008-6215(84)85274-X