N,N-DIETHYL-2-METHYLAMINO-ACETAMIDE HCL

Base Information

• Chemical Name: N,N-DIETHYL-2-METHYLAMINO-ACETAMIDE HCL
• CAS No.: 877880-03-0
• Molecular Formula: C₇H₁₆N₂O*ClH
• Molecular Weight: 180.678
• Mol file: 877880-03-0.mol

Synonyms:

Chemical Property of N,N-DIETHYL-2-METHYLAMINO-ACETAMIDE HCL

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

N,N-Diethyl-2-methylamino-acetamidehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-DIETHYL-2-METHYLAMINO-ACETAMIDE HCL

There total 2 articles about N,N-DIETHYL-2-METHYLAMINO-ACETAMIDE HCL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.4%

tert-butyl N-[(diethylcarbamoyl)methyl]-N-methylcarbamate (934548-21-7) → N,N-diethyl-2-(methylamino)acetamide hydrochloride (877880-03-0)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 6h;

Reference yield:

tert-butyl (2-(diethylamino)-2-oxoethyl)carbamate (500871-60-3) → N,N-diethyl-2-(methylamino)acetamide hydrochloride (877880-03-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.25 h / 20 °C

1.2: 16 h / 20 °C

2.1: hydrogenchloride / 1,4-dioxane / 6 h / 20 °C

With hydrogenchloride; sodium hydride; In tetrahydrofuran; 1,4-dioxane;

upstream raw materials:

tert-butyl (2-(diethylamino)-2-oxoethyl)carbamate

tert-butyl N-[(diethylcarbamoyl)methyl]-N-methylcarbamate

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